1-[3,4-二羟基-5-(羟基甲基)四氢呋喃-2-基]-4,7-二氢-3H-1,3-二氮杂卓-2-酮合成路线 （共 4 条）
反应条件
ammonia in methanol
T=20°C; 30 h;
参考文献
Kim, Minkyoung; Gajulapati, Kondaji; Kim, Chorong; Jung, Hwa Young; Goo, Jail; Lee, Kyeong; Kaur, Navneet; Kang, Hyo Jin; Chung, Sang J.; Choi, Yongseok
Chemical Communications, 2012 , vol. 48, # 93 p. 11443 - 11445
反应条件
1: acetonitrile / 2 h / Ambient temperature
2: HgO, HgBr2 / benzene / 18 h / Heating
3: 85 percent / ammonia / CHCl3; methanol / 24 h / Ambient temperature
View Scheme
参考文献
Liu, Paul S.; Marquez, Victor E.; Driscoll, John S.; Fuller, Richard W.; McCormack, John J.
Journal of Medicinal Chemistry, 1981 , vol. 24, # 6 p. 662 - 666
反应条件
1: HgO, HgBr2 / benzene / 18 h / Heating
2: 85 percent / ammonia / CHCl3; methanol / 24 h / Ambient temperature
View Scheme
参考文献
Liu, Paul S.; Marquez, Victor E.; Driscoll, John S.; Fuller, Richard W.; McCormack, John J.
Journal of Medicinal Chemistry, 1981 , vol. 24, # 6 p. 662 - 666
反应条件
1: 1) BSTFA, 2) HgBr2/HgO
2: NH3 / methanol
View Scheme
参考文献
Liu, Paul S.; Marquez, Victor E.; Kelley, James A.; Driscoll, John S.
Journal of Organic Chemistry, 1980 , vol. 45, # 25 p. 5225 - 5227
