(6S)-6-[(苯甲酰氧基)甲基]-3-氧代-3,6-二氢-2H-吡喃-4-基苯甲酸酯合成路线 （共 6 条）
反应条件
N-bromosuccinmide Irradiation;
参考文献
Lichtenthaler, Frieder W.; Jarglis, Pan; Hempe, Walter
Liebigs Annalen der Chemie, 1983 , # 11 p. 1959 - 1972
反应条件
sodium acetate in acetone
T=25°C; 0.5 h;
参考文献
Brehm, Manfred; Goeckel, Volker H.; Jarglis, Pan; Lichtenthaler, Frieder W.
Tetrahedron Asymmetry, 2008 , vol. 19, # 3 p. 358 - 373
反应条件
1: With pyridine; hydroxylamine hydrochloride
T=70°C; 14 h;
2: With hydrogenchloride; acetaldehyde in acetonitrile
T=20°C; 10 h;
3: With sodium hydrogencarbonate in acetonitrile
6 h; Further stages.;
参考文献
Brehm, Manfred; Goeckel, Volker H.; Jarglis, Pan; Lichtenthaler, Frieder W.
Tetrahedron Asymmetry, 2008 , vol. 19, # 3 p. 358 - 373
反应条件
1: With hydrogenchloride; acetaldehyde in acetonitrile
T=20°C;
2: With sodium hydrogencarbonate in acetonitrile
6 h; Further stages.;
参考文献
Brehm, Manfred; Goeckel, Volker H.; Jarglis, Pan; Lichtenthaler, Frieder W.
Tetrahedron Asymmetry, 2008 , vol. 19, # 3 p. 358 - 373
反应条件
1: 2 N HCl / acetic anhydride; acetonitrile / 10 h / Ambient temperature
2: NaHCO3 / 6 h
View Scheme
参考文献
Brehm, Manfred; Dauben, William G.; Koehler, Peter; Lichtenthaler, Frieder W.
Angewandte Chemie, 1987 , vol. 99, # 12 p. 1318 - 1319
反应条件
in pyridine
T=0 - 20°C;
参考文献
Andersen, Soren M.; Lundt, Inge; Marcussen, Jan; Sotofte; Yu, Shukun
Journal of Carbohydrate Chemistry, 1998 , vol. 17, # 7 p. 1027 - 1035
