(2-溴)六氟-2-(三氟甲基)丙烷合成路线 (共 12 条)
反应条件
sodium iodide in acetonitrile 5 h; Heating;
参考文献
Deev, L. E.; Nazarenko, T. I.; Pashkevich, K.I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1988 , vol. 37, # 2 p. 321 - 323
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1988 , # 2 p. 402 - 404
反应条件
iodine Irradiationmultiple-photon IR laser excitation; different laser frequency and energy fluence; Product distribution;
参考文献
Bagratashvili, V. N.; Kuzmin, M. V.; Letokhov, V. S.
Journal of Physical Chemistry, 1984 , vol. 88, # 24 p. 5780 - 5786
反应条件
iodine Irradiationmultiple-photon IR laser excitation; different laser frequency and energy fluence; Product distribution;
参考文献
Bagratashvili, V. N.; Kuzmin, M. V.; Letokhov, V. S.
Journal of Physical Chemistry, 1984 , vol. 88, # 24 p. 5780 - 5786
反应条件
cesium fluoride in diethylene glycol dimethyl ether
T=20°C; 1.5 h;
参考文献
Zeifman, Yu. V.; Lantseva, L. T.; Postovoi, S. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1981 , vol. 30, # 7 p. 1350 - 1352
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1981 , # 7 p. 1661 - 1663
反应条件
bromine in benzonitrile
参考文献
E. I. Du Pont De Nemours and Company
Patent: US4535184 A1, 1985 ;
参考文献
Bayliff, Andrew E.; Bryce, Martin R.; Chambers, Richard D.; Matthews, Raymond S.
Journal of the Chemical Society, Chemical Communications, 1985 , # 15 p. 1018 - 1019
反应条件
cesium fluoride in diethylene glycol dimethyl ether
1 h; Yields of byproduct given;
参考文献
Postovoi, S. A.; Lantseva, L. T.; Zeifman, Yu. V.; Knunyants, I. L.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, # 11 p. 2233 - 2236
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 11 p. 2531 - 2535
反应条件
bromocyane; silver fluoride
1) acetonitrile, RT, 1 h, 2) 0 deg C, acetonitrile; Yield given. Multistep reaction;
参考文献
Rossman, David E.; Muller, August J.; Lewis, Everett O.
Journal of Fluorine Chemistry, 1991 , vol. 55, # 2 p. 221 - 224
参考文献
Dyatkin,B.L. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1965 , # 10 p. 1833 - 1835
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1965 , # 10 p. 1873 - 1875
反应条件
bromine
T=201°C; 48 h;
参考文献
Tonelli, Claudio; Tortelli, Vito
Journal of Fluorine Chemistry, 1994 , vol. 67, # 2 p. 125 - 128