三甲基(三氟甲基)-锡烷合成路线 （共 52 条）
参考文献
Eujen, R.; Hoge, B.
Journal of Organometallic Chemistry, 1995 , vol. 503, # 2 p. C51 - C54
反应条件
in not given
byproducts: C3F6; absence of air and moisture; heating of Hg-compd. with 2.5 equiv. of SnMe4 (sealed tube, 80°C, 2 weeks); gas chromy.;
参考文献
Eujen, Reint; Lagow, Richard J.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1978 , p. 541 - 544
反应条件
in neat (no solvent)
byproducts: C2F4, c-C3F6; shaken in an ampul (30 min, room temp.); distn.; NMR;
参考文献
Eujen, R.; Thurmann, U.
Journal of Organometallic Chemistry, 1992 , vol. 433, # 1-2 p. 63 - 77
反应条件
educts separately condensed into a reactor held at -196°C, then allowed to react for 15 min at room temp., at 10-fold excess of (CH3)2Cd; volatile products were removed and analyzed, identification by NMR;
参考文献
Krause, L. J.; Morrison, J. A.
Inorganic Chemistry, 1980 , vol. 19, p. 604 - 607
反应条件
in not given
byproducts: Hg, C3F6; absence of air and moisture; heating of Hg-compd. with slight excess of Sn-compd. (sealed tube, 75°C, 1 week); product mixt. not sepd., detd. by (1)H-NMR spectroscopy;
参考文献
Eujen, Reint; Lagow, Richard J.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1978 , p. 541 - 544
参考文献
Bell; Platt
Journal of the Chemical Society [Section] D: Chemical Communications, 1970 , p. 325
View citing articles Show Details
Bell, T. N.; Platt, A. E.
Intern. J. Chem. Kinetics, 1970 , vol. 2, p. 299 - 309
反应条件
T=150°C; 3 h; silica tube in vacuo;
参考文献
Birchall, J. Michael; Fields, Roy; Haszeldine, Robert N.; McLean, Reginald J.
Journal of Fluorine Chemistry, 1980 , vol. 15, p. 487 - 496
反应条件
sodium iodide in ethylene glycol dimethyl ether
参考文献
Seyferth,D. et al.
Journal of the American Chemical Society, 1965 , vol. 87, # 3 p. 681 - 682
Full Text View citing articles Show Details
Seyferth,D. et al.
Journal of Organic Chemistry, 1967 , vol. 32, p. 2980 - 2984
反应条件
benzoic acid in neat (no solvent)
byproducts: C6H5COOCHF2; at 155°C in a sealed tube for 20 h;;
参考文献
Gmelin Handbook: Sn: Org.Verb.2, 1.1.2.1, page 6 - 20
参考文献
Cullen,W.R.; Waldmann,M.C.
Journal of Fluorine Chemistry, 1971 , vol. 1, p. 151
Full Text View citing articles Show Details
Cullen, W. R.; Waldman, M. C.
Inorganic and Nuclear Chemistry Letters, 1968 , p. 205 - 207
