三甲基(三氟甲基)-锡烷合成路线 (共 52 条)
反应条件
(Me2N)2S+Me3SiF2- in Petroleum ether T=25°C; 1.5 h;
参考文献
Kolomeitsev; Movchun; Kondratenko; Yagupolski
Synthesis, 1990 , # 12 p. 1151 - 1152
反应条件
olefine in ethylene glycol dimethyl ether byproducts: NaF; refluxing for 16 h;;
参考文献
Journal of the American Chemical Society, , vol. 87, # 3 p. 681 - 682
Journal of Organic Chemistry, , vol. 32, p. 2980 - 2984
反应条件
sodium iodide in ethylene glycol dimethyl ether byproducts: NaF; refluxing for 16 h;;
参考文献
Journal of Organic Chemistry, , vol. 32, p. 2980 - 2984
反应条件
2) 160 deg C, 3 d; Yield given. Multistep reaction. Further byproducts given;
参考文献
Fritz, Gerhard; Bauer, Heinz
Angewandte Chemie, 1983 , vol. 95, # 9 p. 740 - 741
反应条件
in neat (no solvent) at 150°C for 24 h;;
参考文献
Cullen et al.
Inorganic Chemistry, 1970 , vol. 9, p. 1682,1683, 1684
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Gmelin Handbook: Sn: Org.Verb.2, 1.1.2.1, page 6 - 20
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Waldmann, M. C.
Diss. Abstr. Intern. B, Diss. Univ. of British Columbia 1970 1971 , vol. 31, p. 7174/5
反应条件
in not given reaction in gasphase at 150°C; reaction mechanism discussed;;
参考文献
Cullen et al.
Inorganic Chemistry, 1970 , vol. 9, p. 1682,1683, 1684
反应条件
in neat (no solvent) at 115°C in a sealed tube for 17 h;;
参考文献
Gmelin Handbook: Sn: Org.Verb.2, 1.1.2.1, page 6 - 20
反应条件
in neat (no solvent) at 115°C in a sealed tube for 24 h;;
参考文献
Gmelin Handbook: Sn: Org.Verb.2, 1.1.2.1, page 6 - 20
反应条件
24 h heating at 150°C;
参考文献
Cullen et al.
Inorganic Chemistry, 1970 , vol. 9, p. 1682,1683, 1684
反应条件
in neat (no solvent) byproducts: C2F4, cyclo-C3F6, CHF3; at 115°C in a sealed tube for 18 h;;
参考文献
Gmelin Handbook: Sn: Org.Verb.2, 1.1.2.1, page 6 - 20