Boc-L-天冬氨酸 4-苄酯合成路线 (共 36 条)
反应条件
sodium hydroxide in 1,4-dioxane
参考文献
Tetrahedron Letters, , vol. 32, # 45 p. 6637 - 6640
反应条件
n-octanethiol; tetrabutylammonium fluoride (on alumina) in tetrahydrofuran 0.5 h; Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 34, # 17 p. 2783 - 2786
反应条件
triethylamine in tetrahydrofuran; water 12 h; Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 58, # 9 p. 2369 - 2376
反应条件
piperidine in acetonitrile Ambient temperature;
参考文献
Chemistry of Natural Compounds, , vol. 26, # 2 p. 196 - 198
Khimiya Prirodnykh Soedinenii, , # 2 p. 241 - 245
反应条件
magnesium in methanol T=20°C; 4 h;
参考文献
Synlett, , # 1 art. no. W17911ST, p. 142 - 144
反应条件
1: 98 percent / CuCO3*Cu(OH)2 / ethanol; H2O / 2 h / 70 °C 2: 90 percent / Et3N / H2O; tetrahydrofuran / 12 h / Ambient temperature View Scheme
参考文献
Journal of Organic Chemistry, , vol. 58, # 9 p. 2369 - 2376
反应条件
1: 95 percent / benzene / 3.5 h / Heating 2: 98 percent / CuCO3*Cu(OH)2 / ethanol; H2O / 2 h / 70 °C 3: 90 percent / Et3N / H2O; tetrahydrofuran / 12 h / Ambient temperature View Scheme
参考文献
Journal of Organic Chemistry, , vol. 58, # 9 p. 2369 - 2376
反应条件
1: ethyl acetate / 1 h / Ambient temperature 2: base 3: 91 percent / piperidine / acetonitrile / Ambient temperature View Scheme
参考文献
Chemistry of Natural Compounds, , vol. 26, # 2 p. 196 - 198
Khimiya Prirodnykh Soedinenii, , # 2 p. 241 - 245
反应条件
1: base 2: 91 percent / piperidine / acetonitrile / Ambient temperature View Scheme
参考文献
Chemistry of Natural Compounds, , vol. 26, # 2 p. 196 - 198
Khimiya Prirodnykh Soedinenii, , # 2 p. 241 - 245
反应条件
triethylamine in chloroform; N,N-dimethyl-formamide
参考文献
Chemical and pharmaceutical bulletin, , vol. 15, # 12 p. 2015 - 2016