BOC-L-苯胺-4-硝基苯酯合成路线 （共 21 条）
反应条件
phosphazene; triethylamine in acetonitrile 0.5 h;
参考文献
Vapirov; Tunina
Russian Journal of General Chemistry, 1997 , vol. 67, # 7 p. 1092 - 1094
反应条件
4-methyl-morpholine in tetrahydrofuran 1 h; Ambient temperature;
参考文献
Jaoudai, Mahmoud; Martinez, Jean; Castro, Bertrand
Journal of Organic Chemistry, 1987 , vol. 52, # 12 p. 2364 - 2367
反应条件
1: 75 percent / triethylamine / benzene; light petroleum / 4 h / Ambient temperature 2: 62 percent / N-methylmorpholine / tetrahydrofuran / 1 h / Ambient temperature View Scheme
参考文献
Journal of Organic Chemistry, , vol. 52, # 12 p. 2364 - 2367
反应条件
1: (i), (ii) aq. NaOH, dioxane 2: DCC / ethyl acetate View Scheme
参考文献
Chemische Berichte, , vol. 97, p. 1819 - 1828
反应条件
1: (i), (ii) aq. NaOH, dioxane 2: DCC / ethyl acetate View Scheme
参考文献
Chemische Berichte, , vol. 97, p. 1819 - 1828
参考文献
Chemische Berichte, , vol. 100, p. 3314 - 3318
反应条件
(i), (ii) DCC; Multistep reaction;
参考文献
Journal of the Chemical Society [Section] C: Organic, , p. 689 - 690
反应条件
1: 73 percent 2: 71 percent / aq. NaOH / dioxane View Scheme
参考文献
Van Nispen; Greven
Recueil des Travaux Chimiques des Pays Bas, 1982 , vol. 101, # 12 p. 451 - 455
反应条件
1: 85 percent / aq. 1N NaOH / dioxane / 24 h / Ambient temperature 2: 2N HCl / acetic acid / 0.33 h 3: 1.) 4-hydroxy-3-nitrobenzophenone fixed to a polystyrene matrix, 2.) triethylamine / 2.) DMF, 20 min 4: 2N HCl / acetic acid 5: 1.) 4-hydroxy-3-nitrobenzophenone fixed to a polystyrene matrix, 2.) triethylamine / 2.) DMF, 30 min 6: 85 percent / 2N HCl / acetic acid / 0.5 h View Scheme
参考文献
Grigor'ev, E. I.; Chernova, S. V.
Chemistry of Natural Compounds, 1989 , vol. 25, # 4 p. 468 - 474
反应条件
1: 1) TFA, 2) 1-hydroxybenzotriazole, N-methylmorpholine / 1) O deg C, 10 min, 2) DMF, 2 h 3: 1) 30percent piperidine, 2) TFA, m-cresol / 1) DMF, 12 h, room temperature, 2) 0 deg C, 10 min View Scheme
参考文献
Kalashnikov, V. V.; Samukov, V. V.
Chemistry of Natural Compounds, 1988 , vol. 24, # 3 p. 351 - 354
Khimiya Prirodnykh Soedinenii, 1988 , vol. 24, # 3 p. 412 - 416
