反应条件
1: 88 percent / TFAA, Me2SO, Et3N / CH2Cl2 / -78 °C 2: K-Selectride, KI / diethyl ether / 25 °C 3: 93 percent / HgCl2, HgO / methanol; H2O / Heating 4: 76 percent / hydrogen peroxide / methanol; H2O 5: tetrahydrofuran / Ambient temperature 6: 86 percent / tetrahydrofuran / Ambient temperature 7: HCl / methanol 8: 90 percent / p-carboxybenzenesulfonyl azide, Et3N / acetonitrile / 0 - 20 °C 9: rhodium(II) acetate / benzene / 80 °C 10: DMAP, i-Pr2NEt / acetonitrile / 0 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 102, # 19 p. 6161 - 6163
