L-苯丙氨酸甲酯盐酸盐合成路线 （共 169 条）
反应条件
thionyl chloride in methanol
反应条件
thionyl chloride 1.) from 0 deg C to RT, 100 min, 2.) reflux, 2 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 65, # 2 p. 360 - 365
反应条件
1: With tert.-butylhydroperoxide; cis-(2,2)-Rh2(cap)4 in acetonitrile T=20°C; 16 h; 2: With hydrogenchloride in diethyl ether T=20°C; 6 h;
参考文献
Chemical Communications, , # 7 p. 745 - 747
反应条件
thionyl chloride T=-10 - 20°C; 16 h;
参考文献
European Journal of Medicinal Chemistry, , vol. 68, p. 253 - 259
反应条件
hydrogenchloride in ethyl acetate T=0°C; 2 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 67, # 9 p. 2478 - 2486
反应条件
1: methyl (S)-2-acetamido-3-phenylpropanoate With triphenyl phosphite; chlorine; triethylamine in tetrahydrofuran T=-30°C; 2: 2-methyl-propan-1-ol in tetrahydrofuran T=-30 - 20°C; 3: With water
参考文献
Organic Letters, , vol. 6, # 22 p. 3885 - 3888
反应条件
cesium fluoride in N,N-dimethyl-formamide T=95°C; 10 h;
参考文献
Tetrahedron Letters, , vol. 27, # 19 p. 2099 - 2102
反应条件
1: With thiophenol in N,N-dimethyl-formamide T=20°C; 0.25 h; 2: With hydrogenchloride
参考文献
Synlett, , # 7 p. 1167 - 1169
反应条件
1: With 1,8-diazabicyclo[5.4.0]undec-7-ene; 2-hydroxyethanethiol in N,N-dimethyl-formamide T=20°C; 0.5 h; 2: With hydrogenchloride
参考文献
Synlett, , # 7 p. 1167 - 1169
反应条件
hydrogenchloride in methanol 1 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 71, # 5 p. 2026 - 2036
