1-(4-甲基-2-苯基-1,3-噻唑-5-基)-1-乙酮合成路线 （共 16 条）
反应条件
1: SeO2 / aq. acetic acid / 2 h / Heating 2: 40percent aq. KOH / 24 h / Ambient temperature 3: K2Cr2O7, glacial acetic acid / 1 h View Scheme
参考文献
Simiti; Muresan; Coman
Archiv der Pharmazie, 1981 , vol. 314, # 9 p. 744 - 750
反应条件
in water
T=60°C; 5 h;
参考文献
Kumar, Dalip; Kumar, N. Maruthi; Patel, Gautam; Gupta, Sudeep; Varma, Rajender S.
Tetrahedron Letters, 2011 , vol. 52, # 16 p. 1983 - 1986
反应条件
in ethanol
Hantzsch Thiazole Synthesis; 2 h; Reflux;
参考文献
Tazoo, Dagobert; Oniga, Ovidiu; Bohle, D. Scott; Chua, Zhijie; Dongo, Etienne
Journal of Heterocyclic Chemistry, 2012 , vol. 49, # 4 p. 768 - 773
反应条件
sodium hydroxide
5 h; Ambient temperature;
参考文献
Oehler, Elisabeth; El-Badawi, Mahmoud; Zbiral, Erich
Chemische Berichte, 1985 , vol. 118, # 9 p. 4099 - 4130
参考文献
Prakash; Tyagi; Sangal
Journal of the Indian Chemical Society, 1981 , vol. 57, # 11 p. 1136 - 1137
反应条件
hydrogen iodide in chloroform
参考文献
Csavassy,G.; Gyoerfi,Z.A.
Justus Liebigs Annalen der Chemie, 1974 , p. 1195 - 1205
反应条件
1: 72 percent / 30percent H2O2, Na2CO3 / methanol; H2O / 48 h / 20 °C
2: 39 percent / ethanol / 64 h / Heating
3: 85 percent / 0.5N NaOH / 5 h / Ambient temperature
View Scheme
参考文献
Oehler, Elisabeth; El-Badawi, Mahmoud; Zbiral, Erich
Chemische Berichte, 1985 , vol. 118, # 9 p. 4099 - 4130
反应条件
1: SOCl2 / Heating
2: diethyl ether; benzene
3: aq. HI / CHCl3
View Scheme
参考文献
Csavassy,G.; Gyoerfi,Z.A.
Justus Liebigs Annalen der Chemie, 1974 , p. 1195 - 1205
反应条件
1: KOH / ethanol
2: SOCl2 / Heating
3: diethyl ether; benzene
4: aq. HI / CHCl3
View Scheme
参考文献
Csavassy,G.; Gyoerfi,Z.A.
Justus Liebigs Annalen der Chemie, 1974 , p. 1195 - 1205
反应条件
1: diethyl ether; benzene
2: aq. HI / CHCl3
View Scheme
参考文献
Csavassy,G.; Gyoerfi,Z.A.
Justus Liebigs Annalen der Chemie, 1974 , p. 1195 - 1205
