4,4',4''-[次氮基三(亚甲基)]三[2,6-二(1,1-二甲基乙基)苯酚]合成路线 （共 8 条）
反应条件
1: 90 percent / H2O / acetone / 1) 1h, reflux, 2) after addition of water 1h, reflux 2: 49 percent / 72percent HClO4, H2O / acetone / 28 h / Heating View Scheme
参考文献
Nikiforov, G. A.; Bannikov, G. F.; Mal'donado, I. K. A. Romero; Malysheva, R. D.; Ershov, V. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1989 , vol. <1> 38, # 12 p. 2530 - 2535
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1989 , # 12 p. 2765 - 2770
反应条件
1: 90 percent / H2O / acetone / 1) 1h, reflux, 2) after addition of water 1h, reflux 2: 92 percent / 72percent HClO4 / acetone View Scheme
参考文献
Nikiforov, G. A.; Bannikov, G. F.; Mal'donado, I. K. A. Romero; Malysheva, R. D.; Ershov, V. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1989 , vol. <1> 38, # 12 p. 2530 - 2535
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1989 , # 12 p. 2765 - 2770
反应条件
ammonia in dichloromethane
参考文献
Grinter; Trevor John; Hayler; John David; Negus; Alan; Harris; Michael Anthony
Patent: US6048995 A1, 2000 ;
反应条件
ammonia in water; acetone
0.5 h; Ambient temperature;
参考文献
Bukharov; Nugumanova; Mukmeneva
Russian Journal of General Chemistry, 1998 , vol. 68, # 10 p. 1605 - 1608
反应条件
ammonium hydroxide; Fremy’s salt in acetone
参考文献
Magnusson,R.
Acta Chemica Scandinavica (1947-1973), 1966 , vol. 20, p. 2211 - 2214
反应条件
water in acetone
1) 1h, reflux, 2) after addition of water 1h, reflux;
参考文献
Nikiforov, G. A.; Bannikov, G. F.; Mal'donado, I. K. A. Romero; Malysheva, R. D.; Ershov, V. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1989 , vol. <1> 38, # 12 p. 2530 - 2535
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1989 , # 12 p. 2765 - 2770
反应条件
1: 90 percent / H2O / acetone / 1) 1h, reflux, 2) after addition of water 1h, reflux
2: 96 percent / 72percent HClO4 / 1 h / Heating
View Scheme
参考文献
Nikiforov, G. A.; Bannikov, G. F.; Mal'donado, I. K. A. Romero; Malysheva, R. D.; Ershov, V. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1989 , vol. <1> 38, # 12 p. 2530 - 2535
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1989 , # 12 p. 2765 - 2770
反应条件
1: 90 percent / H2O / acetone / 1) 1h, reflux, 2) after addition of water 1h, reflux
2: 41 percent / 72percent HClO4, H2O / acetone / 28 h / Heating
View Scheme
参考文献
Nikiforov, G. A.; Bannikov, G. F.; Mal'donado, I. K. A. Romero; Malysheva, R. D.; Ershov, V. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1989 , vol. <1> 38, # 12 p. 2530 - 2535
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1989 , # 12 p. 2765 - 2770
