N-叔丁氧羰基-1,3-丙二胺合成路线 （共 26 条）
反应条件
in chloroform 1.) 3 h, ice bath, 2.) room temperature, 16 h;
参考文献
Muller, Dan; Zeltser, Irena; Bitan, Gal; Gilon, Chaim
Journal of Organic Chemistry, 1997 , vol. 62, # 2 p. 411 - 416
反应条件
ammonia; hydrogen; nickel in ethanol T=50°C; P=15514.4 Torr; 8 h;
参考文献
Houssin, Raymond; Bernier, Jean-Luc; Henichart, Jean-Pierre
Synthesis, 1988 , # 3 p. 259 - 261
反应条件
hydrogen; palladium on activated charcoal in ethanol P=1125.09 Torr; 8 h;
参考文献
Benz, Herbert; Hesse, Manfred
Helvetica Chimica Acta, 1993 , vol. 76, # 4 p. 1636 - 1648
反应条件
in tetrahydrofuran T=0 - 20°C; 24 h;
参考文献
APPLIED RESEARCH SYSTEMS ARS HOLDING N.V.
Patent: WO2003/106455 A1, 2003 ;
Location in patent: Page 53-54 ;
WO 03/106455 A1
反应条件
hydrogen; palladium on activated charcoal in ethanol P=2585.7 Torr; 18 h; Ambient temperature;
参考文献
Corrie, John E. T.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 20 p. 2975 - 2982
反应条件
in 1,4-dioxane T=20°C; Inert atmosphere;
参考文献
Bioorganic and Medicinal Chemistry, , vol. 18, # 7 p. 2586 - 2597
参考文献
Tang, Wei; Fang, Shiyue
Tetrahedron Letters, 2008 , vol. 49, # 41 p. 6003 - 6006
反应条件
1: With iodine in methanol T=20°C; 7 h; 2: With zinc in methanol T=20°C; 0.5 h;
参考文献
Vatele, Jean-Michel
Tetrahedron Letters, 2003 , vol. 44, # 51 p. 9127 - 9130
反应条件
sodium chloride in tetrahydrofuran; hydrogenchloride; water; ethyl acetate
参考文献
US5990307 A1, ;
US 5990307 A
反应条件
ammonia in dichloromethane
