N-乙酰-D-氨基葡萄糖合成路线 （共 161 条）
反应条件
trifluoroacetic acid 0.5 h; Ambient temperature;
参考文献
Dondoni, Alessandro; Franco, Santiago; Junquera, Federico; Merchan, Francisco L.; Merino, Pedro; et al.
Chemistry--A European Journal, 1995 , vol. 1, # 8 p. 505 - 520
反应条件
2-acetamido-2-deoxy-5-fluoro-β-D-glucopyranosyl fluoride; NagZ from Vibrio cholerae in various solvent(s) T=37°C; Enzyme kinetics; Further Variations:Reagents;
参考文献
Journal of the American Chemical Society, , vol. 130, # 1 p. 327 - 335
反应条件
N-bromosuccinmide; water in acetone Deacetylation;
参考文献
Wang, Zhi-Guang; Zhang, XuFang; Live, David; Danishefsky, Samuel J.
Angewandte Chemie (International Edition in English), 2000 , vol. 39, # 20 p. X3652-3656
反应条件
1: sodium hydride / dimethylformamide 2: lithium aluminium hydride / diethyl ether / Ambient temperature 3: pyridinium p-toluenesulphonate / H2O; pyridine / Ambient temperature 4: pyridine 5: mercuric chloride-mercuric oxide 6: H2 / 10percent Pd/C / acetic acid / 48 h View Scheme
参考文献
Carbohydrate Research, , vol. 100, p. C5 - C9
反应条件
1: BuLi, Et2AlCl / diethyl ether; hexane / 1.) -78 deg C, 15 min, 2.) -80 deg C, 30 min 2: 20percent aq. TiCl3 / methanol / 0.25 h / Ambient temperature 3: pyridine, DMAP / 12 h / Ambient temperature 5: 80 percent / 80percent aq. TFA / 0.5 h / Ambient temperature View Scheme
参考文献
Chemistry--A European Journal, , vol. 1, # 8 p. 505 - 520
反应条件
1: 2-amino-2-deoxyglucose hydrochloride With sodium in methanol 0.25 h; Inert atmosphere; 2: C6H8N2O5 With pyridine T=20°C; 1 h; Inert atmosphere;
参考文献
RSC Advances, , vol. 4, # 12 p. 6239 - 6245
反应条件
1: 20percent aq. TiCl3 / methanol / 0.25 h / Ambient temperature 2: pyridine, DMAP / 12 h / Ambient temperature 4: 80 percent / 80percent aq. TFA / 0.5 h / Ambient temperature View Scheme
参考文献
Chemistry--A European Journal, , vol. 1, # 8 p. 505 - 520
反应条件
Jack bean N-acetyl-β-D-glucosaminidase in isopropyl alcohol T=37°C; pH=5; 48 h; aq. sodium phosphate bufferEnzymatic reaction;
参考文献
Journal of Medicinal Chemistry, , vol. 54, # 19 p. 6949 - 6955
反应条件
chitin deacetylase from Colletotrichium lindemuthianum in water T=30°C; Deacetylation; pH=8.5; Enzymatic reactionsodium tetraborate/HCl buffer;
参考文献
Carbohydrate Research, , vol. 316, # 1-4 p. 173 - 178
反应条件
chitinase from Streptomyces griseus in phosphate buffer T=30°C; Deacetylation; pH=6.0; 1 h; Enzymatic reaction; Product distribution;
参考文献
Carbohydrate Research, , vol. 316, # 1-4 p. 173 - 178
