4,7-二甲氧基苯并-2,1,3-噻二唑合成路线 （共 3 条）
反应条件
1: With AlCl3, aluminium chloride in toluene 0.75 h; Inert atmosphereReflux; 2: With hydrogenchloride in water; toluene
参考文献
Lei, Ting; Zhou, Yan; Cheng, Chu-Yang; Cao, Yue; Peng, Yang; Bian, Jiang; Pei, Jian
Organic Letters, 2011 , vol. 13, # 10 p. 2642 - 2645
反应条件
1: palladium on carbon; hydrogen / ethyl acetate / 20 °C / 760.05 Torr
2: pyridine; PhNSO / 18 h / Reflux
View Scheme
参考文献
Lei, Ting; Zhou, Yan; Cheng, Chu-Yang; Cao, Yue; Peng, Yang; Bian, Jiang; Pei, Jian
Organic Letters, 2011 , vol. 13, # 10 p. 2642 - 2645
反应条件
1: nitric acid / 3.5 h / 100 °C / Cooling with ice
2: palladium on carbon; hydrogen / ethyl acetate / 20 °C / 760.05 Torr
3: pyridine; PhNSO / 18 h / Reflux
View Scheme
参考文献
Lei, Ting; Zhou, Yan; Cheng, Chu-Yang; Cao, Yue; Peng, Yang; Bian, Jiang; Pei, Jian
Organic Letters, 2011 , vol. 13, # 10 p. 2642 - 2645
