N,N',1,2-四苯基乙烷-1,2-二亚胺合成路线 （共 33 条）
反应条件
anschliessend Behandeln mit wss.Ammoniumchlorid;
参考文献
Garry
Annales de Chimie (Cachan, France), 1942 , vol. <11>17, p. 5,15
Full Text Show Details
Montagne; Garry
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1939 , vol. 208, p. 1735
反应条件
hydrogenchloride in water
T=160°C; 7 h;
参考文献
Van Belzen, Ruud; Klein, Rene A.; Smeets, Wilberth J.J.; Spek, Anthony L.; Benedix, Roland; Elsevier, Cornelis J.
Recueil des Travaux Chimiques des Pays-Bas-Journal of the Royal Netherlands, 1996 , vol. 115, # 5 p. 275 - 285
反应条件
hydrogenchloride in water
T=160°C; 2 h;
参考文献
Van Belzen, Ruud; Klein, Rene A.; Smeets, Wilberth J.J.; Spek, Anthony L.; Benedix, Roland; Elsevier, Cornelis J.
Recueil des Travaux Chimiques des Pays-Bas-Journal of the Royal Netherlands, 1996 , vol. 115, # 5 p. 275 - 285
反应条件
sodium cyanide in N,N-dimethyl-formamide
72 h; Ambient temperature;
参考文献
Singh, Geeta; Mehrotra, Kailash Nath
Heterocycles, 1981 , vol. 16, # 8 p. 1341 - 1344
反应条件
p-benozquinone in dichloromethane
T=25°C; 2 h;
参考文献
Ogle, James W.; Zhang, Jubo; Reibenspies, Joseph H.; Abboud, Khalil A.; Miller, Stephen A.
Organic Letters, 2008 , vol. 10, # 17 p. 3677 - 3680
反应条件
samarium diiodide in tetrahydrofuran
18 h; Heating;
参考文献
Thakur, Ashim J.; Prajapati, Dipak; Sandhu, Jagir S.
Chemistry Letters, 2004 , vol. 33, # 2 p. 102 - 103
参考文献
Strain
Journal of the American Chemical Society, 1929 , vol. 51, p. 272
反应条件
1: 65 percent / K3Fe(CN)6 / benzene; ethanol; H2O / 3.5 h / 70 °C
2: 62 percent / 12M HCl / H2O / 2 h / 160 °C
View Scheme
参考文献
Van Belzen, Ruud; Klein, Rene A.; Smeets, Wilberth J.J.; Spek, Anthony L.; Benedix, Roland; Elsevier, Cornelis J.
Recueil des Travaux Chimiques des Pays-Bas-Journal of the Royal Netherlands, 1996 , vol. 115, # 5 p. 275 - 285
反应条件
1: 92 percent / 12M HCl / H2O / 3 h / 140 °C
2: 65 percent / K3Fe(CN)6 / benzene; ethanol; H2O / 3.5 h / 70 °C
3: 62 percent / 12M HCl / H2O / 2 h / 160 °C
View Scheme
参考文献
Van Belzen, Ruud; Klein, Rene A.; Smeets, Wilberth J.J.; Spek, Anthony L.; Benedix, Roland; Elsevier, Cornelis J.
Recueil des Travaux Chimiques des Pays-Bas-Journal of the Royal Netherlands, 1996 , vol. 115, # 5 p. 275 - 285
反应条件
1: aqueous hydrochloric acid / 140 °C
2: 160 °C / Durchleiten von Sauerstoff
3: aqueous hydrochloric acid / 150 °C
View Scheme
参考文献
Julian et al.
Journal of the American Chemical Society, 1945 , vol. 67, p. 1203,1208
