1,2,3,4-四苯基萘合成路线 （共 86 条）
反应条件
tetrakis(triphenylphosphine) palladium(0); triethylamine in N,N-dimethyl-formamide T=120°C; Suzuki Coupling; 12 h; Inert atmosphere;
参考文献
Singha, Raju; Nandi, Sukla; Ray, Jayanta K.
Tetrahedron Letters, 2012 , vol. 53, # 48 p. 6531 - 6534,4
Title/Abstract Full Text Show Details
Singha, Raju; Nandi, Sukla; Ray, Jayanta K.
Tetrahedron Letters, 2012 , vol. 53, # 48 p. 6531 - 6534
反应条件
sodium carbonate; [RhCl(η2:η2-cycloocta-1,5-diene)]2 in 1,4-dioxane; water T=50°C; 20 h;
参考文献
Harada, Yasuyuki; Nakanishi, Jun; Fujihara, Hirokazu; Tobisu, Mamoru; Fukumoto, Yoshiya; Chatani, Naoto
Journal of the American Chemical Society, 2007 , vol. 129, # 17 p. 5766 - 5771
反应条件
phenyl-magnesium bromide in tetrahydrofuran T=-78°C; 0.166667 h; Inert atmosphere;
参考文献
Yoshida, Suguru; Uchida, Keisuke; Hosoya, Takamitsu
Chemistry Letters, 2014 , vol. 43, # 1 p. 116 - 118
反应条件
potassium tetrachloropalladate; sodium acetate in neat (no solvent) T=80°C; 3 h; Inert atmosphereGreen chemistry; regioselective reaction;
参考文献
Bej, Ansuman; Chakraborty, Amarnath; Sarkar, Amitabha
RSC Advances, 2013 , vol. 3, # 36 p. 15812 - 15819
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran; dichloromethane T=20°C; cycloaddition; elimination; 0.5 h;
参考文献
Kitamura, Tsugio; Yamane, Masakatsu; Inoue, Kensuke; Todaka, Mitsuru; Fukatsu, Norihiko; Meng, Zhaohong; Fujiwara, Yuzo
Journal of the American Chemical Society, 1999 , vol. 121, # 50 p. 11674 - 11679
反应条件
silver carbonate; [{(η5-C5Me5)IrCl}2(μ-Cl)2] in xylene T=160°C; 6 h;
参考文献
Ueura, Kenji; Satoh, Tetsuya; Miura, Masahiro
Journal of Organic Chemistry, 2007 , vol. 72, # 14 p. 5362 - 5367
反应条件
copper diacetate; [RhCl(η2:η2-cycloocta-1,5-diene)]2 in o-xylene T=170°C; 4 h;
参考文献
Uto, Toshihiko; Shimizu, Masaki; Ueura, Kenji; Tsurugi, Hayato; Satoh, Tetsuya; Miura, Masahiro
Journal of Organic Chemistry, 2008 , vol. 73, # 1 p. 298 - 300
反应条件
[{(η5-C5Me5)RhCl}2(μ-Cl)2]; air; copper (II) acetate monohydrate in N,N-dimethyl-formamide T=100°C; 2 h;
参考文献
Fukutani, Tatsuya; Hirano, Koji; Satoh, Tetsuya; Miura, Masahiro
Journal of Organic Chemistry, 2011 , vol. 76, # 8 p. 2867 - 2874
反应条件
Ni(Br)2(dppe); 1,2-bis-(diphenylphosphino)ethane; zinc in acetonitrile T=100°C; 48 h; Inert atmosphere;
参考文献
Hsieh, Jen-Chieh; Cheng, Chien-Hong
Chemical Communications, 2008 , # 26 p. 2992 - 2994
反应条件
Ni(Br)2(dppe); 1,2-bis-(diphenylphosphino)ethane; zinc in acetonitrile T=100°C; 48 h; Inert atmosphere;
参考文献
Hsieh, Jen-Chieh; Cheng, Chien-Hong
Chemical Communications, 2008 , # 26 p. 2992 - 2994
