1,3,5-三(4-甲氧基苯基)苯合成路线 (共 29 条)
反应条件
sodium carbonate; palladium diacetate in water; N,N-dimethyl-formamide T=60°C; Suzuki; 12 h;
参考文献
Liu, Leifang; Zhang, Yuhong; Xin, Bingwei
Journal of Organic Chemistry, 2006 , vol. 71, # 10 p. 3994 - 3997
反应条件
bis(allyl)-ruthenium(IV) dimer in methanol; water T=75°C; 24 h;
参考文献
Journal of the American Chemical Society, , vol. 128, # 47 p. 15094 - 15095
反应条件
TiCl3(OTf) T=90 - 100°C; 10 h;
参考文献
Iranpoor; Zeynizaded
Synlett, 1998 , # 10 p. 1079 - 1080
反应条件
palladium diacetate; triphenylphosphine in tetrahydrofuran T=110°C; 6 h; Inert atmosphere;
参考文献
Tetrahedron, , vol. 67, # 38 p. 7386 - 7391
反应条件
indium(III) chloride; 2-iodophenol in chlorobenzene 24 h; Reflux; regioselective reaction;
参考文献
Xu, Yan-Li; Pan, Ying-Ming; Wu, Qiang; Wang, Heng-Shan; Liu, Pei-Zhen
Journal of Organic Chemistry, 2011 , vol. 76, # 20 p. 8472 - 8476
反应条件
toluene-4-sulfonic acid in neat (no solvent) T=60 - 140°C; 11 h; Green chemistry; regioselective reaction;
参考文献
Gao, Qi; Bao, Fang-Ping; Feng, Xiao-Jing; Pan, Ying-Ming; Wang, Heng-Shan; Li, Dian-Peng
Arkivoc, 2013 , vol. 2013, # 3 p. 49 - 60
反应条件
Cp2Zr(OSO2C8H17)2 in toluene T=110°C; 3 h; chemoselective reaction;
参考文献
Zhang, Guo Ping; Qiu, Ren Hua; Xu, Xin Hua; Zhou, Hai Hui; Kuang, Ya Fei; Chen, Si Hai
Synthetic Communications, 2012 , vol. 42, # 6 p. 858 - 864
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in tetrahydrofuran Heating;
参考文献
Pena, Miguel A.; Perez, Ignacio; Perez Sestelo, Jose; Sarandeses, Luis A.
Chemical Communications, 2002 , # 19 p. 2246 - 2247
反应条件
Sm(III) chloride; acetyl chloride in pentane 2 h; Ambient temperature;
参考文献
Cheng, Ke-Jun; Ding, Zong-Biao; Wu, Shi-Hui
Synthetic Communications, 1997 , vol. 27, # 1 p. 11 - 15
反应条件
tetrakis(triphenylphosphine) palladium(0); cesium fluoride in tetrahydrofuran Suzuki coupling; 48 h; RefluxInert atmosphere;
参考文献
Iannazzo, Laura; Vollhardt, K. Peter C.; Malacria, Max; Aubert, Corinne; Gandon, Vincent
European Journal of Organic Chemistry, 2011 , # 18 p. 3283 - 3292