4’-溴-2-羟基苯乙酮乙酸酯合成路线 (共 28 条)
反应条件
1: 7-methoxy-4-methyl-3,4-dihydrocoumarin With Catalyst M-Chromium oxide in water
Oxidation; 2 h; Heating;
2: 2-bromo-1-(4-bromophenyl)-1-ethanone in ethanol
Acetoxylation; 0.666667 h; Heating;
参考文献
Raj; Kapil; Bhaumik; Mahesh
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 1999 , vol. 38, # 7 p. 759 - 762
反应条件
sodium ethanolate in ethanol
参考文献
Kaspersen, Svein Jacob; Hoff, Bard Helge; Sundby, Eirik; Charnock, Colin
Bioorganic Chemistry, 2012 , vol. 44, p. 35 - 41,7
反应条件
in acetonitrile
3 h; Heating;
参考文献
Kamal, Ahmed; Sandbhor, Mahendra; Ahmed, Kaleem; Adil; Shaik, Ahmad Ali
Tetrahedron Asymmetry, 2003 , vol. 14, # 24 p. 3861 - 3866
反应条件
in dimethyl sulfoxide
Ambient temperature;
参考文献
Nozaki,H. et al.
Bulletin of the Chemical Society of Japan, 1972 , vol. 45, p. 856 - 859
参考文献
Achenbach, Hans; Boettger-Vetter, Angelika; Hunkler, Dieter; Fautz, Erich; Reichenbach, Hans
Tetrahedron, 1983 , vol. 39, # 1 p. 175 - 186
反应条件
formic acid
T=180°C; 20 h;
参考文献
Yordanova; Shvedov; Dantchev
Chemische Berichte, 1982 , vol. 115, # 7 p. 2635 - 2642
反应条件
1: glacial acetic acid / 0.5 h / 180 °C
2: HCOOH / 5.5 h / 180 °C
View Scheme
参考文献
Yordanova; Shvedov; Dantchev
Chemische Berichte, 1982 , vol. 115, # 7 p. 2635 - 2642
反应条件
sodium tetrahydroborate in methanol
T=20°C;
参考文献
Kamal, Ahmed; Chouhan, Gagan
Tetrahedron Letters, 2004 , vol. 45, # 48 p. 8801 - 8805