1,2-二溴-1,1-二氟乙烷合成路线 (共 11 条)
反应条件
bromine; acetic acid
参考文献
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 843,848;engl.Ausg.S.863,868
反应条件
bromine tris(fluorosulfate) T=30°C; 3 h;
参考文献
Fokin, A. V.; Studnev, Yu. N.; Rapkin, A. I.; Chilikin, V. G.; Verenikin, O. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1985 , vol. 34, # 3 p. 601 - 607
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1985 , # 3 p. 659 - 665
反应条件
tetrakis(triphenylphosphine) palladium(0); chloro-trimethyl-silane; diiodomethane; zinc 1.) THF, 60-90 deg C, 30 min, 2.) THF, 60 deg C, 4 h; Yield given. Multistep reaction. Further byproducts given;
参考文献
Journal of Organic Chemistry, , vol. 62, # 22 p. 7758 - 7764
参考文献
Industrial and Engineering Chemistry, , vol. 39, p. 421
Journal of the American Chemical Society, , vol. 69, p. 946
参考文献
Chemisches Zentralblatt, , p. II,804
参考文献
Chem. Zentralbl., , vol. 82, # II p. 848
参考文献
Swarts
Chem. Zentralbl., 1911 , vol. 82, # II p. 848
反应条件
diethyl ether; phenyl-magnesium bromide
参考文献
Bulletin de la Societe Chimique de France, , vol. <4>25, p. 168
参考文献
Capriel,P.; Binsch,G.
Tetrahedron, 1979 , vol. 35, p. 2661 - 2668
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Demiel,A.
Journal of Organic Chemistry, 1960 , vol. 25, p. 993 - 996
反应条件
Zersetzen des Reaktionsproduktes mit Wasser;
参考文献
Swarts
Bulletin de la Societe Chimique de France, 1919 , vol. <4>25, p. 168