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乙二醇
甲醛
63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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氟里昂-22
合成路线
（共 327 条）
75-45-6
氟里昂-22
→
反应条件
885132-71-8
反应条件
potassium carbonate in N,N-dimethyl-formamide T=100°C; Alkylation; 3 h;
参考文献
Yamanaka; Moritomo; Fujii; Tanaka; Fukuda; Nishimura
Pesticide Science, 1998 , vol. 54, # 3 p. 223 - 229
75-45-6
氟里昂-22
+
100-53-8
苄硫醇
→
反应条件
68965-44-6
反应条件
potassium hydroxide in water T=60°C; P=760.051 Torr; 4 h; Product distribution / selectivity;
参考文献
Saint-Jalmes, Laurent
Patent: US2006/178536 A1, 2006 ;
Location in patent: Page/Page column 4-5 ;
75-45-6
氟里昂-22
+
538-28-3
S-苄基异硫脲盐酸盐
→
反应条件
68965-44-6
反应条件
1: 2-benzyl-2-thiopseudourea hydrochloride With potassium hydroxide; tetrabutylammomium bromide in water; toluene T=60°C; 0.666667 h; 2: 1-chloro-1,1-difluoro-methane With potassium hydroxide in water; toluene T=40°C; 4.7 h; Product distribution / selectivity;
参考文献
Ihara Chemical Industry Co., Ltd.
Patent: JP2005/112810 A, 2005 ;
Location in patent: Page/Page column 8 ;
75-45-6
氟里昂-22
+
106-99-0
丁二烯
→
反应条件
694-34-8
1,1-二氟-2-乙烯基环丙烷
反应条件
tetrabutylammomium bromide; hydroquinone in various solvent(s) T=120°C; P=15001.2 Torr;
参考文献
Gassen, K. R.; Baasner, B.
Journal of Fluorine Chemistry, 1990 , vol. 49, # 1 p. 127 - 139
75-45-6
氟里昂-22
+
2581-34-2
4-硝基间甲苯酚
→
反应条件
795303-16-1
反应条件
sodium hydroxide in 1,4-dioxane; water T=70°C; 0.5 h;
参考文献
RICERCA BIOSCIENCES, LLC.
Patent: WO2004/99162 A1, 2004 ;
Location in patent: Page 37-38 ;
75-45-6
氟里昂-22
+
1122-91-4
→
反应条件
84750-93-6
反应条件
tetrabutyl-ammonium chloride; triphenylphosphine; methyloxirane in N,N-dimethyl-formamide T=110°C; Wittig Olefination; 6 h; Sealed tubeMolecular sieveInert atmosphere; SolventConcentrationTemperatureTime;
参考文献
Zheng, Jian; Lin, Jin-Hong; Cai, Ji; Xiao, Ji-Chang
Chemistry - A European Journal, 2013 , vol. 19, # 45 p. 15261 - 15266
75-45-6
氟里昂-22
+
454-89-7
→
反应条件
90605-29-1
反应条件
tetrabutyl-ammonium chloride; triphenylphosphine; methyloxirane in N,N-dimethyl-formamide T=110°C; Wittig Olefination; 6 h; Sealed tubeMolecular sieveInert atmosphere;
参考文献
Zheng, Jian; Lin, Jin-Hong; Cai, Ji; Xiao, Ji-Chang
Chemistry - A European Journal, 2013 , vol. 19, # 45 p. 15261 - 15266
288-13-1
+
75-45-6
氟里昂-22
→
反应条件
908014-77-7
反应条件
potassium hydroxide in diethylene glycol dimethyl ether; water T=90 - 100°C;
参考文献
Petko; Sokolenko; Yagupolskii
Chemistry of Heterocyclic Compounds, 2006 , vol. 42, # 9 p. 1177 - 1184
288-32-4
+
75-45-6
氟里昂-22
→
反应条件
91459-68-6
反应条件
dibenzo-18-crown-6; potassium hydroxide in ethylene glycol dimethyl ether; water Heating;
参考文献
Levterov, Vadym; Grygorenko, Oleksandr O.; Mykhailiuk, Pavel K.; Tolmachev, Andrey A.
Synthesis, 2011 , # 8 art. no. N50310SS, p. 1243 - 1248
75-45-6
氟里昂-22
+
149-30-4
→
反应条件
943-08-8
反应条件
1: 1-chloro-1,1-difluoro-methane With potassium hydroxide in ethylene glycol dimethyl ether; water 0.166667 h; 2: 2-mercaptobenzothiazole in ethylene glycol dimethyl ether; water T=20°C; Inert atmosphere;
参考文献
Zhao, Yanchuan; Huang, Weizhou; Zhu, Lingui; Hu, Jinbo
Organic Letters, 2010 , vol. 12, # 7 p. 1444 - 1447
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