in tetrahydrofuran addn. of CH2Cl2 to soln. of B-methoxyborecane in THF, cooling to -78°C, slow addn. of sec-BuLi over period of 0.5 h, stirred at -78°C for 0.25 h, addn. of KIPBH, warmed to room temp, stirred for 14 h;; GLC, amt. of cyclodecanol formed depends upon temp. during the addn. of KIPBH;;
参考文献
Brown, Herbert C.; Phadke, Avinash S.; Rangaishenvi, Milind V.
Journal of the American Chemical Society, 1988 , vol. 110, # 18 p. 6263 - 6264
in dichloromethane Irradiation (UV/VIS); N2-atmosphere; laser flash photolysis into wavelength of MCLT band of title compd.; not isolated, reaction followed by transient UV/VIS spectroscopy;
参考文献
Rossenaar, Brenda D.; Lindsay, Elspeth; Stufkens, Derk J.; Vlcek Jr., Antonin
Inorganica Chimica Acta, 1996 , vol. 250, # 1-2 PART I p. 5 - 14
Abel, Edward W.; Orrell, Keith G.; Rahoo, Haji; Sik, Vladimir; Mazid, Mohammed A.; Hursthouse, Michael B.
Journal of Organometallic Chemistry, 1992 , vol. 437, # 1/2 p. 191 - 199
