双(2,4-二硝基苯基)碳酸脂合成路线 (共 8 条)
反应条件
in tetrahydrofuran T=60°C; 49 h; Product distribution / selectivity;
参考文献
JSR Corporation
Patent: US2007/15932 A1, 2007 ;
Location in patent: Page/Page column 5 ;
参考文献
Jost, Philippe; Forestiere, Alain; Sillion, Bernard; Le Perchec, Pierre
Tetrahedron Letters, 1982 , vol. 23, # 42 p. 4311 - 4314
反应条件
potassium acetate T=156 - 186°C;
参考文献
Witt,H. et al.
Angewandte Chemie, 1970 , vol. 82, p. 79 - 80
反应条件
in water; acetonitrile T=20 - 45°C; pH-independent hydrolysis in MeCN-H2O mixtures; ΔH(act.), ΔS(act.), ΔG(act.); various binary solvent compositions; effect H2O mole fraction; hydrolysis in MeCN-H2O-D2O mixtures; structure of transition state; solute-solvent interaction mechanism; Rate constantThermodynamic dataKinetics;
参考文献
El Seoud, Omar A.; El Seoud, Monica I.; Farah, Joao P.S.
Journal of Organic Chemistry, 1997 , vol. 62, # 17 p. 5928 - 5933
参考文献
Kempf
Journal fuer Praktische Chemie (Leipzig), 1870 , vol. <2> 1, p. 412
Jahresbericht ueber die Fortschritte der Chemie und Verwandter Theile Anderer Wissenschaften, 1870 , p. 396
反应条件
N,N-dimethyl-aniline; benzene
参考文献
Raiford; Inman
Journal of the American Chemical Society, 1934 , vol. 56, p. 1586,1587
反应条件
sulfuric acid; nitric acid
参考文献
Kempf
Journal fuer Praktische Chemie (Leipzig), 1870 , vol. <2> 1, p. 412
Jahresbericht ueber die Fortschritte der Chemie und Verwandter Theile Anderer Wissenschaften, 1870 , p. 396
反应条件
in toluene
6 h; Ambient temperature;
参考文献
El Seoud, Omar A.; El Seoud, Monica I.; Farah, Joao P.S.
Journal of Organic Chemistry, 1997 , vol. 62, # 17 p. 5928 - 5933