4-硝基苯基-α-D-吡喃半乳糖苷合成路线 （共 19 条）
反应条件
1: stannic tetrachloride / CH2Cl2 / 5 h / 60 °C 2: 1 M sodium methoxide / methanol View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 59, p. 314 - 320
反应条件
methanol; sodium methylate
参考文献
Justus Liebigs Annalen der Chemie, , vol. 589, p. 77,79
Hoppe-Seyler's Zeitschrift fuer Physiologische Chemie, , vol. 311, p. 54,58
反应条件
1: dichloromethyl methyl ether, boron trifluoride 2: 40 percent / hexamethylphosphoric acid triamide / 40 deg C, 6 h; r.t. 3: 1 M sodium methoxide / methanol View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 59, p. 314 - 320
反应条件
1: 40 percent / hexamethylphosphoric acid triamide / 40 deg C, 6 h; r.t. 2: 1 M sodium methoxide / methanol View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 59, p. 314 - 320
反应条件
1: mercury (II)-cyanide 2: sodium methylate; methanol View Scheme
参考文献
Justus Liebigs Annalen der Chemie, , vol. 589, p. 77,79
Hoppe-Seyler's Zeitschrift fuer Physiologische Chemie, , vol. 311, p. 54,58
反应条件
1: recombinant Aspergillus nidulans FGSC GH36 α-galactosidase / 3 h / 37 °C / pH 5 / aq. acetate buffer; Enzymatic reaction 2: recombinant Aspergillus nidulans FGSC GH36 α-galactosidase / 1 h / 37 °C / pH 5 / aq. acetate buffer; Enzymatic reaction View Scheme
参考文献
Nakai, Hiroyuki; Baumann, Martin J.; Petersen, Bent O.; Westphal, Yvonne; Hachem, Maher Abou; Dilokpimol, Adiphol; Duus, Jens .; Schols, Henk A.; Svensson, Birte
FEBS Journal, 2010 , vol. 277, # 17 p. 3538 - 3551
反应条件
recombinant Aspergillus nidulans FGSC GH36 α-galactosidase T=37°C; pH=5; 3 h; aq. acetate bufferEnzymatic reaction; regioselective reaction;
参考文献
Nakai, Hiroyuki; Baumann, Martin J.; Petersen, Bent O.; Westphal, Yvonne; Hachem, Maher Abou; Dilokpimol, Adiphol; Duus, Jens .; Schols, Henk A.; Svensson, Birte
FEBS Journal, 2010 , vol. 277, # 17 p. 3538 - 3551
反应条件
1: recombinant Aspergillus nidulans FGSC GH36 α-galactosidase / 3 h / 37 °C / pH 5 / aq. acetate buffer; Enzymatic reaction 2: recombinant Aspergillus nidulans FGSC GH36 α-galactosidase / 1 h / 37 °C / pH 5 / aq. acetate buffer; Enzymatic reaction View Scheme
参考文献
Nakai, Hiroyuki; Baumann, Martin J.; Petersen, Bent O.; Westphal, Yvonne; Hachem, Maher Abou; Dilokpimol, Adiphol; Duus, Jens .; Schols, Henk A.; Svensson, Birte
FEBS Journal, 2010 , vol. 277, # 17 p. 3538 - 3551
反应条件
6(A),6(D)-di-C-cyano(hydroxy)methyl-β-cyclodextrin; water T=59°C; pH=8; 6 h; aq. phosphate buffer; Kinetics; Reagent/catalystConcentration; chemoselective reaction;
参考文献
Bjerre, Jeannette; Bols, Mikael
European Journal of Organic Chemistry, 2010 , # 18 p. 3487 - 3500
反应条件
1: recombinant Aspergillus nidulans FGSC GH36 α-galactosidase / 3 h / 37 °C / pH 5 / aq. acetate buffer; Enzymatic reaction 2: recombinant Aspergillus nidulans FGSC GH36 α-galactosidase / 1 h / 37 °C / pH 5 / aq. acetate buffer; Enzymatic reaction View Scheme
参考文献
Nakai, Hiroyuki; Baumann, Martin J.; Petersen, Bent O.; Westphal, Yvonne; Hachem, Maher Abou; Dilokpimol, Adiphol; Duus, Jens .; Schols, Henk A.; Svensson, Birte
FEBS Journal, 2010 , vol. 277, # 17 p. 3538 - 3551
