2-吡啶-2-基喹啉-4-羧酸合成路线 (共 23 条)
反应条件
1: Na / hexamethylphosphoric acid triamide / 48 h / 80 °C
2: mCPBA / CHCl3 / Ambient temperature
3: 54 percent / MeMgBr / tetrahydrofuran / 0.25 h / Ambient temperature
View Scheme
参考文献
Wakabayashi, Shoji; Kubo, Yukihiro; Takeda, Takashi; Uenishi, Jun-ichi; Oae, Shigeru
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 7 p. 2338 - 2341
反应条件
1: mCPBA / CHCl3 / Ambient temperature
2: 54 percent / MeMgBr / tetrahydrofuran / 0.25 h / Ambient temperature
View Scheme
参考文献
Wakabayashi, Shoji; Kubo, Yukihiro; Takeda, Takashi; Uenishi, Jun-ichi; Oae, Shigeru
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 7 p. 2338 - 2341
反应条件
1: N,N-dimethylcarbamoyl chloride / dichloromethane / 0 °C
2: η5-cyclopentadienyl-η4-cycloocta-1,5-diene-cobalt(I) / toluene / 120 °C
View Scheme
参考文献
Zucca, Antonio; Cordeschi, Diletta; Maidich, Luca; Pilo, Maria Itria; Masolo, Elisabetta; Stoccoro, Sergio; Cinellu, Maria Agostina; Galli, Simona
Inorganic Chemistry, 2013 , vol. 52, # 13 p. 7717 - 7731