(1R,2S)-1-氨基-2-茚满醇合成路线 （共 78 条）
反应条件
1: H2SO4 conc. / 3 h / 20 °C 2: 2.67 g / aq. H2SO4 / acetonitrile / 8 h / 50 °C View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 12, # 1 p. 59 - 62
反应条件
1: HONH2, HCl 2: H2, HBr / Pd-black View Scheme
参考文献
Tetrahedron Letters, , vol. 39, # 43 p. 7921 - 7924
反应条件
1: 68 percent / H2O / 48 h / 30 - 35 °C / baker's yeast 2: 57 percent / 1 M aq.NaOH / 1 h / Ambient temperature 3: 29 percent / diphenylphosphoryl azide (DPPA), Et3N / Heating 4: 80.6 percent / SOCl2 / Ambient temperature 5: 82.5 percent / aq.KOH / ethanol / 24 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 47, # 27 p. 4941 - 4958
反应条件
1: 57 percent / 1 M aq.NaOH / 1 h / Ambient temperature 2: 29 percent / diphenylphosphoryl azide (DPPA), Et3N / Heating 3: 80.6 percent / SOCl2 / Ambient temperature 4: 82.5 percent / aq.KOH / ethanol / 24 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 47, # 27 p. 4941 - 4958
反应条件
1: 29 percent / diphenylphosphoryl azide (DPPA), Et3N / Heating 2: 80.6 percent / SOCl2 / Ambient temperature 3: 82.5 percent / aq.KOH / ethanol / 24 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 47, # 27 p. 4941 - 4958
反应条件
potassium hydroxide; sulfuric acid; acetonitrile Yield given. Multistep reaction;
参考文献
Tetrahedron Asymmetry, , vol. 7, # 6 p. 1559 - 1562
反应条件
hydrogenchloride; hydrogen; palladium in methanol 20 h; Ambient temperatureeffect of acid, effect of catalyst, effect of hydrogen pressure, effect of solvent; Product distribution;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 72, # 5 p. 1093 - 1100
反应条件
1: 83 percent / acetone / 1 h / Heating 2: 76 percent / aq. NaOH / 1 h / Heating View Scheme
参考文献
Shukla, Upendra K.; Singh, Raieshwar; Khanna, J. M.; Saxena, Anil K.; Singh, Hemant K.; et al.
Collection of Czechoslovak Chemical Communications, 1992 , vol. 57, # 2 p. 415 - 424
反应条件
in acetone 1 h; Heating;
参考文献
Shukla, Upendra K.; Singh, Raieshwar; Khanna, J. M.; Saxena, Anil K.; Singh, Hemant K.; et al.
Collection of Czechoslovak Chemical Communications, 1992 , vol. 57, # 2 p. 415 - 424
反应条件
sodium hydroxide; [Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2 in isopropyl alcohol
参考文献
Brands, Karel M. Jos; Payack, Joseph F.; Pye, Philip J.
Patent: US2002/52493 A1, 2002 ;
