4,4-亚乙烯双(N,N-二甲基苯胺)合成路线 (共 18 条)
反应条件
1: Methyltriphenylphosphonium bromide With potassium tert-butylate in tetrahydrofuran T=0°C; 2 h; Inert atmosphere; 2: 4,4'-bis-(N,N-dimethylamino)-benzophenone in tetrahydrofuran T=0°C; Wittig Olefination; Reflux;
参考文献
Wu, Lingling; Wang, Yanshai; Wang, Yurong; Shen, Kaihua; Li, Yang
Polymer (United Kingdom), 2013 , vol. 54, # 12 p. 2958 - 2965
反应条件
sodium hydroxide; poly(ethylene glycol) 2000; palladium diacetate in water T=150°C; Hiyama reaction; 2 h;
参考文献
Gordillo, Alvaro; De Jesus, Ernesto; Lopez-Mardomingo, Carmen
Chemical Communications, 2007 , # 39 p. 4056 - 4058
反应条件
sodium hydroxide in benzene
参考文献
Kanzaki Paper Manufacturing Co., Ltd.
Patent: US4898941 A1, 1990 ;
反应条件
magnesium in diethyl ether; benzene
参考文献
Takasago Perfumery Co., Ltd.
Patent: US4751163 A1, 1988 ;
反应条件
sodium hydroxide; palladium diacetate in water T=140°C; 5 h;
参考文献
Gordillo, Alvaro; De Jesus, Ernesto; Lopez-Mardomingo, Carmen
Chemical Communications, 2007 , # 39 p. 4056 - 4058
参考文献
Matsui, Masaki; Tsuge, Michinori; Shibata, Katsuyoshi; Muramatsu, Hiroshige
Bulletin of the Chemical Society of Japan, 1994 , vol. 67, # 6 p. 1753 - 1755
反应条件
methyl-magnesium iodide
参考文献
Justus Liebigs Annalen der Chemie, , vol. 461, p. 145
参考文献
Journal of Organic Chemistry, , vol. 23, p. 1056
参考文献
Journal of Organic Chemistry, , vol. 23, p. 1056
参考文献
Gollnick, Klaus; Schnatterer, Albert; Utschick, Gerald
Journal of Organic Chemistry, 1993 , vol. 58, # 22 p. 6049 - 6056