反应条件
in hydrogenchloride
byproducts: KCl; N2, 50°C, several h, exclusion of light;; evapd.; titurated with DMF; decanted from KCl; addn. of acetone; ppt. fitered off; washed with acetone and dry Et2O; dried under vacuum over Drierite;;
参考文献
Howell, B. A.; Walles, E. W.
Inorganica Chimica Acta, 1988 , vol. 142, p. 185 - 186
