lithium iodide in various solvent(s) T=130°C; 5 h; Yield given;
参考文献
Barreiro, Eliezer J.; Costa, Paulo R. R.; Barros, Perola Regina V. R.; Queiroz, Waldemir M.
Journal of Chemical Research, Miniprint, 1982 , # 4 p. 1142 - 1165
peracetic acid in chloroform
72 h; Ambient temperature;
参考文献
Barreiro, Eliezer J.; Costa, Paulo R. R.; Barros, Perola Regina V. R.; Queiroz, Waldemir M.
Journal of Chemical Research, Miniprint, 1982 , # 4 p. 1142 - 1165
n-butyllithium
1) in hexane, tetrahydrofuran, -78 deg C, 5 min 2) 0.5 h, -78 deg C, then -10 deg C; Yield given. Multistep reaction. Further byproducts given. Title compound not separated from byproducts;
参考文献
Sanghvi, Y. S.; Dabral, V.; Bhat, K. S.; Rao, A. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 1 p. 12 - 14
n-butyllithium
1) in hexane, tetrahydrofuran, -78 deg C, 5 min 2) 0.5 h, -78 deg C, then -10 deg C; Multistep reaction. Further byproducts given. Title compound not separated from byproducts;
参考文献
Sanghvi, Y. S.; Dabral, V.; Bhat, K. S.; Rao, A. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 1 p. 12 - 14
hydrogen; palladium on activated charcoal in methanol
P=3361.5 Torr; 3 h;
参考文献
Barreiro, Eliezer J.; Costa, Paulo R. R.; Barros, Perola Regina V. R.; Queiroz, Waldemir M.
Journal of Chemical Research, Miniprint, 1982 , # 4 p. 1142 - 1165
