4-氨基-N-(2-吡啶基)苯甲酰胺合成路线 (共 4 条)
反应条件
hydrogen; palladium 10 on activated carbon in 1,4-dioxane; methanol P=760.051 Torr; 24 h;
参考文献
COUNCIL OF SCIENTIFIC AND INDUSTRIAL RESEARCH; INDIAN INSTITUTE OF CHEMICAL TECHNOLOGY; Yadav, Jhillu S.; Lavanya, Madugula; Das, Pragna P.; Krishnan, Anita; Jagannadh, Bulusu; Pal-Bhadra, Manika; Bhadra, Utpal
Patent: US2013/52137 A1, 2013 ;
Location in patent: Paragraph 0057; 0058 ;
反应条件
1: CHCl3; pyridine 2: platinum; acetic acid / Hydrogenation View Scheme
参考文献
Chemische Berichte, , vol. 75, p. 711,716
反应条件
1.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 0 - 20 °C / Inert atmosphere 1.2: 0 °C 2.1: hydrogen / palladium 10 on activated carbon / 1,4-dioxane; methanol / 24 h / 760.05 Torr View Scheme
反应条件
1: CHCl3; pyridine 2: platinum; acetic acid / Hydrogenation View Scheme
参考文献
Chemische Berichte, , vol. 75, p. 711,716