(1-甲基-1H-苯并咪唑-2-基)甲醇合成路线 (共 18 条)
反应条件
diisobutylaluminium hydride in tetrahydrofuran; hexane T=0°C; 1 h;
参考文献
Bioorganic and Medicinal Chemistry, , vol. 14, # 19 p. 6695 - 6712
反应条件
sulfuric acid; silver nitrate in methanol; water 3 h; Heating;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 18, # 12 p. 1299 - 1302
Khimiya Geterotsiklicheskikh Soedinenii, , vol. 18, # 12 p. 1679 - 1681
反应条件
tetrabutylammomium bromide; potassium hydroxide in tetrahydrofuran T=0°C;
参考文献
Bulletin of the Korean Chemical Society, , vol. 34, # 4 p. 1272 - 1274
反应条件
sodium hydroxide in methanol T=20°C; 0.5 h;
参考文献
Synthetic Communications, , vol. 37, # 10 p. 1675 - 1681
反应条件
hydrogenchloride Heating;
参考文献
Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical & Analytical, , vol. 25, # 12 p. 1092 - 1096
反应条件
in water 1.5 h; Reflux;
参考文献
Journal of Chemical Sciences, , vol. 125, # 6 p. 1555 - 1571
反应条件
1: 2 h / 125 - 130 °C 2: water / Heating 3: 75 percent / TEBAC; K2CO3 / acetonitrile / 20 °C 4: 76 percent / aq. NaOH / methanol / 0.5 h / 20 °C View Scheme
参考文献
Synthetic Communications, , vol. 37, # 10 p. 1675 - 1681
反应条件
1: hydrogenchloride / water / 6 h / Reflux 2: tetrabutylammomium bromide; potassium hydroxide / tetrahydrofuran / 0 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 22, # 2 p. 933 - 936
反应条件
methanol; sodium hydroxide
参考文献
Journal and Proceedings of the Royal Society of New South Wales, , vol. 71, p. 209,221
反应条件
1: 75 percent / TEBAC; K2CO3 / acetonitrile / 20 °C 2: 76 percent / aq. NaOH / methanol / 0.5 h / 20 °C View Scheme
参考文献
Synthetic Communications, , vol. 37, # 10 p. 1675 - 1681