N-苯基-4-甲氧基苯甲酰胺合成路线 （共 11 条）
反应条件
[RuIII(2,4-pentanedionato)3]; methanesulfonic acid; hydrogen; 1,1,1-tris (diphenylphosphinomethyl)ethane in tetrahydrofuran T=200°C; P=7500.75 Torr; 16 h; AutoclaveInert atmosphere;
参考文献
Coetzee, Jacorien; Dodds, Deborah L.; Klankermayer, Juergen; Brosinski, Sandra; Leitner, Walter; Slawin, Alexandra M. Z.; Cole-Hamilton, David J.
Chemistry - A European Journal, 2013 , vol. 19, # 33 p. 11039 - 11050
反应条件
titanium tetrachloride; magnesium in tetrahydrofuran T=0 - 20°C; Inert atmosphere;
参考文献
Zhang, Tongxin; Zhang, Yan; Zhang, Weixi; Luo, Meiming
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 14-15 p. 2775 - 2780
反应条件
[RuIII(2,4-pentanedionato)3]; methanesulfonic acid; hydrogen; 1,1,1-tris (diphenylphosphinomethyl)ethane in tetrahydrofuran T=200°C; P=7500.75 Torr; 16 h; AutoclaveInert atmosphere;
参考文献
Coetzee, Jacorien; Dodds, Deborah L.; Klankermayer, Juergen; Brosinski, Sandra; Leitner, Walter; Slawin, Alexandra M. Z.; Cole-Hamilton, David J.
Chemistry - A European Journal, 2013 , vol. 19, # 33 p. 11039 - 11050
反应条件
40 potassium fluoride/alumina 0.0666667 h; Microwave irradiationNeat (no solvent);
参考文献
Chinese Journal of Chemistry, , vol. 29, # 10 p. 2209 - 2212
反应条件
potassium phosphate; copper(l) iodide; N-methyl-2-(methylamino)ethylamine in toluene T=130°C; 24 h; Inert atmosphere;
参考文献
Racine, Emilie; Monnier, Florian; Vors, Jean-Pierre; Taillefer, Marc
Organic Letters, 2011 , vol. 13, # 11 p. 2818 - 2821
反应条件
trichlorophosphate Behandeln des Reaktionsproduktes mit verd. Saeure;
参考文献
Hoechster Farbw.
Patent: DE295495 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 13, p. 339
参考文献
Shah; Deshpande; Chaubal
Journal of the Chemical Society, 1932 , p. 642,645
反应条件
1: 80 percent / TMEDA, n-BuLi / hexane; tetrahydrofuran / 1.) -78 deg C to -20 deg C, 2 h, 2.) room temperature, overnight
2: 1.) NBS, benzoylperoxide, 2.) AlCl3 / 1.) CCl4, irradiation, reflux, overnight, 2.) CH3NO2, room temperature, 1 h
View Scheme
参考文献
Sartori; Bigi; Tao; Porta; Maggi; Predieri; Lanfranchi; Pellinghelli
Journal of Organic Chemistry, 1995 , vol. 60, # 20 p. 6588 - 6591
反应条件
n-butyllithium; N,N,N',N,-tetramethylethylenediamine in tetrahydrofuran; hexane
1.) -78 deg C to -20 deg C, 2 h, 2.) room temperature, overnight;
参考文献
Sartori; Bigi; Tao; Porta; Maggi; Predieri; Lanfranchi; Pellinghelli
Journal of Organic Chemistry, 1995 , vol. 60, # 20 p. 6588 - 6591
反应条件
oxygen; copper(II) bis(trifluoromethanesulfonate) in o-xylene
T=140°C; P=760.051 Torr; 28 h;
参考文献
Ueda, Satoshi; Nagasawa, Hideko
Angewandte Chemie - International Edition, 2008 , vol. 47, # 34 p. 6411 - 6413
