N,N-二乙基-4-甲氧基-苯甲酰胺合成路线 （共 48 条）
反应条件
in dichloromethane
T=0 - 20°C; 2.25 h;
参考文献
White, Jonathan M.; Tunoori, Ashok Rao; Turunen, Brandon J.; Georg, Gunda I.
Journal of Organic Chemistry, 2004 , vol. 69, # 7 p. 2573 - 2576
反应条件
1: 0.08 h / Heating
2: 72 percent / NiCl2(PPh3)2 / tetrahydrofuran / 2 h / 20 °C
View Scheme
参考文献
Lemoucheux; Rouden; Lasne
Tetrahedron Letters, 2000 , vol. 41, # 51 p. 9997 - 10001
反应条件
1: H2O; methanol / 4 h / Ambient temperature
2: 78 percent / 50percent aq. NaOH, benzyltriethylammonium chloride, O2 / dimethylsulfoxide / 4 h
View Scheme
参考文献
Yuste, Francisco; Origel, Alfredo E.; Brena, Leonardo J.
Synthesis, 1983 , # 2 p. 109 - 110
反应条件
mercury dibromide in toluene
12 h; Heatingvar. solv.;
参考文献
Fujiwara, Shin-Ichi; Ogawa, Akiya; Kambe, Nobuaki; Ryu, Ilhyong; Sonoda, Noboru
Tetrahedron Letters, 1988 , vol. 29, # 47 p. 6121 - 6124
反应条件
pyridine in dichloromethane
Substitution; 20 h;
参考文献
Keck, Gary E; McLaws, Mark D; Wager, Travis T
Tetrahedron, 2000 , vol. 56, # 51 p. 9875 - 9883
反应条件
1: 4-Methoxy-thiobenzoic acid S-(5,5-dimethyl-2-thioxo-2λ5-[1,3,2]dioxaphosphinan-2-yl) ester in benzene
1 h; Heating;
2: diethylamine in benzene
cooling; Further stages.;
参考文献
Doszczak, Leszek; Rachon, Janusz
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 10 p. 1271 - 1279
反应条件
in acetonitrile
2 h; Ambient temperature; Yield given;
参考文献
Kikukawa, Kiyoshi; Kono, Kiyoshi; Nagira, Kazuhiko; Wada, Fumio; Matsuda, Tsutomu
Journal of Organic Chemistry, 1981 , vol. 46, p. 4413 - 4416
反应条件
1: benzene / Behandeln des Reaktionsprodukts mit wss. Natronlauge
2: aq. NaOH solution
View Scheme
参考文献
Couturier
Annales de Chimie (Cachan, France), 1938 , vol. <11> 10, p. 559,597
参考文献
Couturier
Annales de Chimie (Cachan, France), 1938 , vol. <11> 10, p. 559,597
反应条件
bis(cyclopentadienyl) zirconium chloride deuteride in tetrahydrofuran
T=20°C; 0.25 h;
参考文献
Spletstoser, Jared T.; White, Jonathan M.; Tunoori, Ashok Rao; Georg, Gunda I.
Journal of the American Chemical Society, 2007 , vol. 129, # 11 p. 3408 - 3419
