N,N-二乙基-4-甲氧基-苯甲酰胺合成路线 （共 48 条）
反应条件
triethylamine; Pd-bis(1-methylbenzothiazole-2-carbene) in N,N-dimethyl acetamide
T=130°C; 7 h;
参考文献
Calo, Vincenzo; Giannoccaro, Potenzo; Nacci, Angelo; Monopoli, Antonio
Journal of Organometalic Chemistry, 2002 , vol. 645, # 1-2 p. 152 - 157
反应条件
triethylamine in benzene
0.25 h;
参考文献
Doszczak, Leszek; Rachon, Janusz
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 10 p. 1271 - 1279
反应条件
4-(4,6-Dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholin-4-ium chloride in tetrahydrofuran
3 h;
参考文献
TOKUYAMA CORPORATION
Patent: EP1178043 A1, 2002 ;
Location in patent: Page 20, 22 ;
反应条件
mercury dibromide in various solvent(s)
12 h; Heating;
参考文献
Fujiwara, Shin-Ichi; Ogawa, Akiya; Kambe, Nobuaki; Ryu, Ilhyong; Sonoda, Noboru
Tetrahedron Letters, 1988 , vol. 29, # 47 p. 6121 - 6124
反应条件
triethylamine in dichloromethane
T=20°C; 1 h;
参考文献
Kang, Dong Ho; Joo, Tae Young; Lee, Eun Hwa; Chaysripongkul, Skaydaw; Chavasiri, Warinthorn; Jang, Doo Ok
Tetrahedron Letters, 2006 , vol. 47, # 32 p. 5693 - 5696
反应条件
Amberlyst A-21
Acylation;
参考文献
Girard; Tranchant; Niore; Herscovici
Synlett, 2000 , # 11 p. 1577 - 1580
反应条件
1: 71 percent / K2CO3 / dimethylformamide / 2 h / 25 °C
2: 1.) Al(CH3)3 / 1.) benzene, toluene, 1 h, 25 deg C, 2.) 75 deg C, 40 h
3: 11 percent / tetrahydrofuran; diethyl ether / 0.02 h / -65 °C
View Scheme
参考文献
Patterson, John W.
Journal of Organic Chemistry, 1995 , vol. 60, # 14 p. 4542 - 4548
反应条件
1: 1.) Al(CH3)3 / 1.) benzene, toluene, 1 h, 25 deg C, 2.) 75 deg C, 40 h
2: 11 percent / tetrahydrofuran; diethyl ether / 0.02 h / -65 °C
View Scheme
参考文献
Patterson, John W.
Journal of Organic Chemistry, 1995 , vol. 60, # 14 p. 4542 - 4548
反应条件
in tetrahydrofuran; diethyl ether
T=-65°C; 0.0166667 h;
参考文献
Patterson, John W.
Journal of Organic Chemistry, 1995 , vol. 60, # 14 p. 4542 - 4548
反应条件
1: Pd(OAc)2 / acetonitrile / 0.5 h / 6619.6 Torr / Ambient temperature
2: acetonitrile / 2 h / Ambient temperature
View Scheme
参考文献
Kikukawa, Kiyoshi; Kono, Kiyoshi; Nagira, Kazuhiko; Wada, Fumio; Matsuda, Tsutomu
Journal of Organic Chemistry, 1981 , vol. 46, p. 4413 - 4416
