N,N-二乙基-4-甲氧基-苯甲酰胺合成路线 （共 48 条）
反应条件
1: With disodium hydrogenphosphate in acetonitrile T=20°C; Methylation; 2: With disodium hydrogenphosphate Hydrolysis; 18 h;
参考文献
Keck, Gary E; McLaws, Mark D; Wager, Travis T
Tetrahedron, 2000 , vol. 56, # 51 p. 9875 - 9883
反应条件
samarium diiodide; water; triethylamine in tetrahydrofuran T=23°C; 18 h; Inert atmosphere; chemoselective reaction;
参考文献
Szostak, Michal; Spain, Malcolm; Eberhart, Andrew J.; Procter, David J.
Journal of the American Chemical Society, 2014 , vol. 136, # 6 p. 2268 - 2271
反应条件
diethyl ether; benzene
参考文献
Annales de Chimie (Cachan, France), , vol. <11> 10, p. 559,597
反应条件
anschliessendes Behandeln mit wss. Salzsaeure;
参考文献
Annales de Chimie (Cachan, France), , vol. <11> 10, p. 559,597
反应条件
4-(4,6-Dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholin-4-ium chloride in methanol
4 h;
参考文献
TOKUYAMA CORPORATION
Patent: EP1178043 A1, 2002 ;
Location in patent: Page 20, 22 ;
反应条件
triethylamine in N,N-dimethyl acetamide
T=130°C; P=15001.5 Torr; 1.5 h; AutoclaveGreen chemistry; Catalytic behavior;
参考文献
Mei, Hui; Hu, Jianglin; Xiao, Se; Lei, Yizhu; Li, Guangxing
Applied Catalysis A: General, 2014 , vol. 475, p. 40 - 47
反应条件
1: in tetrahydrofuran
T=-78 - 20°C; 0.666667 h; Inert atmosphere;
2: With oxygen; potassium hexamethylsilazane in tetrahydrofuran; toluene
T=-78 - 20°C; 12 h;
参考文献
Wang, Xinbo; Wang, David Zhigang
Tetrahedron, 2011 , vol. 67, # 19 p. 3406 - 3411
反应条件
bis-triphenylphosphine-palladium(II) chloride; octyne-4; water; triethylamine in benzene
T=130°C; P=15200 Torr; 24 h;
参考文献
Coperet, Christophe; Sugihara, Takumichi; Wu, Guangzhong; Shimoyama, Izumi; Negishi, Ei-Ichi
Journal of the American Chemical Society, 1995 , vol. 117, # 12 p. 3422 - 3431
反应条件
bis-triphenylphosphine-palladium(II) chloride; water; triethylamine in benzene
T=130°C; P=15200 Torr; 24 h;
参考文献
Coperet, Christophe; Sugihara, Takumichi; Wu, Guangzhong; Shimoyama, Izumi; Negishi, Ei-Ichi
Journal of the American Chemical Society, 1995 , vol. 117, # 12 p. 3422 - 3431
反应条件
bis-triphenylphosphine-palladium(II) chloride; octyne-4; water in benzene
T=130°C; P=15200 Torr; 24 h;
参考文献
Coperet, Christophe; Sugihara, Takumichi; Wu, Guangzhong; Shimoyama, Izumi; Negishi, Ei-Ichi
Journal of the American Chemical Society, 1995 , vol. 117, # 12 p. 3422 - 3431
