9-羟基-萘嵌苯-1-酮合成路线 （共 11 条）
反应条件
sodium hydroxide; potassium permanganate in water Heating;
参考文献
Koelsch; Anthes
Journal of Organic Chemistry, 1941 , vol. 6, p. 558,563
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in tetrahydrofuran 24 h; Ambient temperature;
参考文献
Olekhnovich, L. P.; Voloshin, N. A.; Tikhonova, M. E.; Borisenko, N. I.; Zhdanov, Yu. A.; Minkin, V. I.
Journal of Organic Chemistry USSR (English Translation), 1990 , vol. 26, # 3.1 p. 399 - 407
Zhurnal Organicheskoi Khimii, 1990 , vol. 26, # 3 p. 466 - 476
反应条件
aluminium trichloride in 1,2-dichloro-ethane
1) ca. 0 deg C to room temperature, ca. 1 h, 2) reflux, 3 h;
参考文献
Haddon, R. C.; Rayford, R.; Hirani, A. M.
Journal of Organic Chemistry, 1981 , vol. 46, # 22 p. 4587 - 4588
反应条件
oxygen in tetrahydrofuran
T=20°C; 0.333333 h; IrradiationRose Bengal, sens.;
参考文献
Weeratunga, Gamini; Austrup, Mona; Rodrigo, Russell
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 3169 - 3174
反应条件
1: 95 percent / NaBH4 / methanol / 3 h / Ambient temperature
2: DDQ / benzene / 18 h / Heating
3: 71 percent / O2 / tetrahydrofuran / 0.33 h / 20 °C / Irradiation; Rose Bengal, sens.
View Scheme
参考文献
Weeratunga, Gamini; Austrup, Mona; Rodrigo, Russell
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 3169 - 3174
反应条件
1: DDQ / benzene / 18 h / Heating
2: 71 percent / O2 / tetrahydrofuran / 0.33 h / 20 °C / Irradiation; Rose Bengal, sens.
View Scheme
参考文献
Weeratunga, Gamini; Austrup, Mona; Rodrigo, Russell
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 3169 - 3174
反应条件
1: 80 percent / CDI / benzene / 24 h / Heating
2: 71 percent / O2 / tetrahydrofuran / 0.33 h / 20 °C / Irradiation; Rose Bengal, sens.
View Scheme
参考文献
Weeratunga, Gamini; Austrup, Mona; Rodrigo, Russell
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 3169 - 3174
反应条件
sodium methylate
Behandeln des Reaktionsprodukts mit wss.H2SO4;
参考文献
Silberman; Silberman
Austral.J.Sci., 1956 , vol. 19, p. 115
参考文献
Loudon; Razdan
Journal of the Chemical Society, 1954 , p. 4299,4301
反应条件
1: 80 percent / conc. NH4OH / 1 h / 125 °C / 9050.09 Torr
2: 81 percent / 1,2-dichloro-ethane
3: 55 percent / NH3 / ethanol / 2 h
View Scheme
参考文献
Haddon, R. C.; Chichester, S. V.; Mayo, S. L.
Synthesis, 1985 , # 6/7 p. 639 - 641
