1H-吡唑-3,5-二甲酰氯合成路线 （共 9 条）
反应条件
1: K2CO3 / acetone / 1 h / Heating 2: 68 percent / aq. H2SO4 / 18 h / Heating 3: SOCl2 / 0.5 h / Heating View Scheme
参考文献
Lee, Ho H.; Cain, Bruce F.; Denny, William A.; Buckleton, John S.; Clark, George R.
Journal of Organic Chemistry, 1989 , vol. 54, # 2 p. 428 - 431
反应条件
potassium carbonate in acetone 1 h; Heating; Yield given;
参考文献
Lee, Ho H.; Cain, Bruce F.; Denny, William A.; Buckleton, John S.; Clark, George R.
Journal of Organic Chemistry, 1989 , vol. 54, # 2 p. 428 - 431
反应条件
1: K2CO3 / acetone / 1 h / Heating 2: 68 percent / aq. H2SO4 / 18 h / Heating View Scheme
参考文献
Lee, Ho H.; Cain, Bruce F.; Denny, William A.; Buckleton, John S.; Clark, George R.
Journal of Organic Chemistry, 1989 , vol. 54, # 2 p. 428 - 431
反应条件
1: K2CO3 / acetone / 1 h / Heating 2: 89 percent / KOH / methanol / 24 h / 20 °C 3: SOCl2 / 0.5 h / Heating View Scheme
参考文献
Lee, Ho H.; Cain, Bruce F.; Denny, William A.; Buckleton, John S.; Clark, George R.
Journal of Organic Chemistry, 1989 , vol. 54, # 2 p. 428 - 431
反应条件
1: K2CO3 / acetone / 1 h / Heating 2: 89 percent / KOH / methanol / 24 h / 20 °C View Scheme
参考文献
Lee, Ho H.; Cain, Bruce F.; Denny, William A.; Buckleton, John S.; Clark, George R.
Journal of Organic Chemistry, 1989 , vol. 54, # 2 p. 428 - 431
反应条件
thionyl chloride
T=140°C; 2 h;
参考文献
Reviriego, Felipe; Navarro, Pilar; Aran, Vicente J.; Jimeno, Maria Luisa; Garcia-Espana, Enrique; Latorre, Julio; Yunta, Maria J. R.
Journal of Organic Chemistry, 2011 , vol. 76, # 20 p. 8223 - 8231
反应条件
1: 47 percent / KMnO4 / H2O / Heating
2: thionyl chloride / methanol / 24 h / Heating
View Scheme
参考文献
Lee, Ho H.; Cain, Bruce F.; Denny, William A.; Buckleton, John S.; Clark, George R.
Journal of Organic Chemistry, 1989 , vol. 54, # 2 p. 428 - 431
反应条件
1: HCl
2: Cl2SO
View Scheme
参考文献
Elguero, J.; Navarro, P.; Franco, M. I. Rodriguez
Chemistry Letters, 1984 , p. 425 - 428
参考文献
Eidebenz; Koulen
Archiv der Pharmazie (Weinheim, Germany), 1943 , vol. 281, p. 171,180
