sulfuric acid; hydrogen; palladium on activated charcoal in ethanol
P=1292.9 Torr; Ambient temperature;
参考文献
Kiong, Lam Soot; Tyman, John H. P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 1942 - 1952
Kiong, Lam Soot; Tyman, John H. P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 1942 - 1952
Halim, Haroen; Locksley, Harry D.; Memon, Janmohammed J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2331 - 2337
1: 78 g / bromine, red mercuric oxide / various solvent(s) / 3 h / 80 - 90 °C
2: 22 percent / butyl-lithium / hexane; tetrahydrofuran / 4 h / Heating
3: 70 percent / butyl-lithium / hexane; tetrahydrofuran; hexamethylphosphoric acid triamide / 24 h / Ambient temperature
4: 0.4 g / hydrogen / 5percent palladium-barium sulphate / ethyl acetate
View Scheme
参考文献
Halim, Haroen; Locksley, Harry D.; Memon, Janmohammed J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2331 - 2337
Halim, Haroen; Locksley, Harry D.; Memon, Janmohammed J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2331 - 2337