2-羟基-3-甲氧基-5-甲基苯甲醛合成路线 (共 14 条)
反应条件
boric acid; glycerol
T=150°C; Behandeln des auf 110grad abgekuehlten Reaktionsgemisches mit wss.H2SO4;
参考文献
Fuson; Gaertner; Chadwick
Journal of Organic Chemistry, 1948 , vol. 13, p. 489,493
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Manske; Ledingham
Canadian Journal of Research, Section B: Chemical Sciences, 1944 , vol. 22, p. 115,123
反应条件
sodium hydroxide; water in chloroform
T=65 - 75°C; 4 h; other reagent, other temperature, other time; Product distribution;
参考文献
Matoba, Katsuhide; Kawagoshi, Fujiko; Yamazaki, Takao
Chemical & Pharmaceutical Bulletin, 1984 , vol. 32, # 12 p. 4721 - 4725
反应条件
tin(ll) chloride in 1,4-dioxane
Heating; Yield given;
参考文献
Sinhababu, Achintya K.; Borchardt, Ronald T.
Synthetic Communications, 1983 , vol. 13, # 8 p. 677 - 684
参考文献
Tiemann; Koppe
Chemische Berichte, 1881 , vol. 14, p. 2021
参考文献
Ohmori, Hidenobu; Matsumoto, Akiteru; Masui, Masaichiro
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1980 , p. 347 - 357
反应条件
1: aqueous HCl; toluene; amalgamated zinc
2: glycerol; boric acid / 150 °C / Behandeln des auf 110grad abgekuehlten Reaktionsgemisches mit wss.H2SO4
View Scheme
参考文献
Manske; Ledingham
Canadian Journal of Research, Section B: Chemical Sciences, 1944 , vol. 22, p. 115,123
反应条件
sodium hydroxide; dihydrogen peroxide; iron(III) cation
T=80°C; Oxidation; decomposition; 2 h; Product distribution; Further Variations:other metal ions; also without metal ion;
参考文献
Sun, Yujun; Fenster, Michael; Yu, Annie; Berry, Richard M.; Argyropoulos, Dimitris S.
Canadian Journal of Chemistry, 1999 , vol. 77, # 5-6 p. 667 - 675
反应条件
hydrogen; palladium on activated charcoal in ethanol
参考文献
Arnarp; Bielawski; Dahlin; Dahlman; Enzell; Pettersson
Acta chemica Scandinavica (Copenhagen, Denmark : 1989), 1989 , vol. 43, # 1 p. 44 - 50
反应条件
sodium perchlorate; sodium acetate in acetic acid; acetonitrile
Ambient temperatureanodic oxidation in controlled pot. electrolysis, 0.80 V;
参考文献
Ohmori, Hidenobu; Matsumoto, Akiteru; Masui, Masaichiro
Chemical & Pharmaceutical Bulletin, 1980 , vol. 28, # 6 p. 1887 - 1891
参考文献
Browne; Shriner
Journal of Organic Chemistry, 1957 , vol. 22, p. 1320