in neat (no solvent) absence of moisture; large excess AlCl3, evacuated quartz tube, 573 K; fractional sublimation over 450 to 650 K gradient, removal of residual AlCl3 on heating in Cl2/N2 stream;
Brown; Marvel
Journal of the American Chemical Society, 1937 , vol. 59, p. 1176
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Marvel; Himel
Journal of the American Chemical Society, 1940 , vol. 62, p. 1550,1552