in neat (no solvent) exclusion of moisture; heating (573 K, 40 h) in a sealed tube; sepn. of dichlorophosphate, isolation of AlCl3*POCl3 on partial evapn.;
Gmelin Handbook: Al: MVol.B1, 6.3.2.1, page 179 - 181
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Gniadeck, B.
Dissert. Muenchen T. H. 1913, p. 81
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Gniadeck, B.
Dissert. Muenchen T. H. 1913, p.74