13-乙基-3-甲氧基雌甾-1,3,5(10),8-四烯-17b-醇合成路线 （共 15 条）
反应条件
lithium aluminium tetrahydride in diethyl ether 0.0833333 h; Ambient temperatureultrasound;
参考文献
Quinkert; Del Grosso; Doring; Schenkel; Bauch; Dambacher; Bats; Zimmermann; Durner
Helvetica Chimica Acta, 1995 , vol. 78, # 5 p. 1345 - 1391
反应条件
1: triethylenediamine / xylene 2: aq. HCl / methanol 3: NaBH4 / methanol 4: H2 / Raney-Ni / dioxane 5: Py 6: KOH / methanol View Scheme
参考文献
Chemical and pharmaceutical bulletin, , vol. 13, # 11 p. 1289 - 1294
反应条件
1: NaBH4 / methanol 2: H2 / Raney-Ni / dioxane 3: Py 4: KOH / methanol View Scheme
参考文献
Chemical and pharmaceutical bulletin, , vol. 13, # 11 p. 1289 - 1294
反应条件
1: aq. HCl / methanol 2: NaBH4 / methanol 3: H2 / Raney-Ni / dioxane 4: Py 5: KOH / methanol View Scheme
参考文献
Chemical and pharmaceutical bulletin, , vol. 13, # 11 p. 1289 - 1294
反应条件
1: H2 / Raney-Ni / dioxane 2: Py 3: KOH / methanol View Scheme
参考文献
Chemical and pharmaceutical bulletin, , vol. 13, # 11 p. 1289 - 1294
反应条件
1: H2 / Pd-CaCO3 / benzene; tetrahydrofuran 2: KOH / methanol View Scheme
参考文献
Justus Liebigs Annalen der Chemie, , vol. 702, p. 141 - 148
反应条件
potassium hydroxide in methanol
参考文献
Chemical and pharmaceutical bulletin, , vol. 13, # 11 p. 1289 - 1294
反应条件
potassium hydroxide in methanol
参考文献
Justus Liebigs Annalen der Chemie, , vol. 702, p. 141 - 148
反应条件
1: 75 percent / NH3 liq., Li / propan-2-ol; tetrahydrofuran / -45 °C 2: 85 percent / Py*SO3 / dimethylsulfoxide; triethylamine / Ambient temperature 3: 92 percent / oxalic acid, silica gel / CH2Cl2; methanol; H2O / 0.25 h / Ambient temperature View Scheme
参考文献
Lui, Li-Gong; Zhang, Tong; Li, Zhen-Su
Synthetic Communications, 1996 , vol. 26, # 16 p. 2999 - 3006
反应条件
1: 75 percent / NH3 liq., Li / propan-2-ol; tetrahydrofuran / -45 °C 2: 85 percent / Py*SO3 / dimethylsulfoxide; triethylamine / Ambient temperature View Scheme
参考文献
Rufer,C. et al.
Justus Liebigs Annalen der Chemie, 1967 , vol. 702, p. 141 - 148
