in solid pyrolysis at 430-700°C, 10E-3-10E-4 torr, in a He stream;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 38, # 6.2 p. 1308 - 1312
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 6 p. 1428 - 1432
in diethylene glycol dimethyl ether byproducts: MgCl2; under N2 atm. using Schlenk techniques; Mg2Ge added to dried (<30 ppm H2O); mixt. stirred and heated to reflux (about 155-160°C) overnight under N2; GeCl4 (3-fold excess) added to stirred suspn.; after a few min Ge was obtained; monitored by XAS/EXAFS spectroscopy;
参考文献
Journal of Solid State Chemistry, , vol. 184, # 9 p. 2345 - 2352
in gas byproducts: ethane, ethene; Irradiation (UV/VIS); laser-induced photolytic chemical vapour deposition (LPCVD) of (C2H5)2GeH2 (2.7 kPa) at 193 nm and deposition of Ge on a reactor NaCl window;; IR and energy-dispersive X-ray spectroscopy;;
参考文献
Journal of the Chemical Society, Faraday Transactions, , vol. 88, # 12 p. 1637 - 1642
in solid pyrolysis at 430-700°C, 10E-3-10E-4 torr, in a He stream;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 38, # 6.2 p. 1308 - 1312
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 6 p. 1428 - 1432
