反应条件
in neat (no solvent) byproducts: C70, C84; preparing dispersed particels of carbon black by Ar jet crushing; vaporizing C6H6 and carrying by an Ar stream; introduction of starting materials into the hot plasma zone of reactor, >6000K, Ar atmosphere; detailed description of apparatus given;; extracting the combined formed compounds with toluene (Soxhlet), concg. of toluene soln., 90°C, N2; heating under vacuum, 10E-5Torr, 200°C, 6h; main product: C60, further fullerens could be detected (MS);;
参考文献
Yoshie, Ken-ichi; Kasuya, Shigeaki; Eguchi, Keisuke; Yoshida, Toyonobu
Applied Physics Letters, 1992 , vol. 61, p. 2782 - 2783
