反应条件
in neat (no solvent) chlorination (fused silica reactor, 773, 973, 1173, and 1373 K, Cl2 velocity 1 cm/s); removal of Cl2 and TiCl4 on heat treatment (synthesis temp., vac., 1 h);
参考文献
Journal of Applied Chemistry USSR (English Translation), , vol. 55, p. 40 - 43
Zhurnal Prikladnoi Khimii (Sankt-Peterburg, Russian Federation), , vol. 55, p. 46 - 50