反应条件
in hexane byproducts: ((CH3)3Si)2NH, (CH3)3SiOSi(CH3)3, (CH3)3SiNCS; (Ar); soln. of tin complex in hexane was placed in bomb at -100°C, OCS was added, stirred and warmed to 25°C, stirred overnight; cooled to -78°C excess OCS was removed in vac., filtered, washed with pentane, crystal were obtained from filtrate, elem. anal.;
参考文献
Stewart, Constantine A.; Dickie, Diane A.; Parkes, Marie V.; Saria, Josephat A.; Kemp, Richard A.
Inorganic Chemistry, 2010 , vol. 49, # 23 p. 11133 - 11141
