clay in neat (no solvent) reaction in a vacuum at 1450 °C;;
参考文献
Zintl, E.; Braeuning, W.; Grube, H. L.; Krings, W.; Morawietz, W.
Z. Anorg. Chem., 1940 , vol. 245, p. 1 - 7
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Gmelin Handbook: Si: MVol.B, 50, page 127 - 129
in gaseous matrix Kinetics; flow of reactants in N2 was heated at 325-800°C in quartz tube with graphite plate at 510**(-4) Torr; detd. by IR spectroscopy;
参考文献
Ojeda; Abel; Albella
Journal of Physical Chemistry B, 2002 , vol. 106, # 24 p. 6258 - 6264