反应条件
sodium chloride in melt Electrochem. Process; anode: graphite crucible with melt (49percent NaCl, 49percent Na3AlF6, 1percent Na2MoO4, 1percent SiO2), cathode: W rod, reference electrode: Pt wire, 900°C, 1.0A/cm**2, 10 min; product removing with cathode, mixture crushing, leaching (water and aq.H2SO4 at 50-60°C), solid residue sepn. and drying (100-105.degre e.C);
参考文献
Russian Journal of Inorganic Chemistry, , vol. 41, # 12 p. 1888 - 1892