反应条件
in tetrahydrofuran FeCl3 in THF was added dropwise to stirring soln. of 12 ml LiBEt3H in THF (1.0 M), held at const. temp. under N2 atm.; forms of particles dependon dropping rate (1 drop/10s, 1/s, 2/s), stirring rate (200, 400, 1600 rpm) and temp.(0 - 60°C); vac. filtration, washed THF/EtOH (1:1), dried in vac.;
参考文献
Takeuchi, Kenneth J.; Marschilok, Amy C.; Bessel, Carol A.; Dollahon, Norman R.
Journal of Catalysis, 2002 , vol. 208, # 1 p. 150 - 157
