叔丁基(4-甲基苯基)硫醚合成路线 （共 21 条）
反应条件
anhydrous iron chloride; potassium tert-butylate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in 1,4-dioxane
T=135°C; 24 h; Inert atmosphere;
参考文献
Wu, Jhih-Ru; Lin, Che-Hung; Lee, Chin-Fa
Chemical Communications, 2009 , # 29 p. 4450 - 4452
反应条件
CyPF-tBu; palladium diacetate; sodium t-butanolate in ethylene glycol dimethyl ether
T=90°C; 5 h; Inert atmosphere;
参考文献
Fernandez-Rodriguez, Manuel A.; Hartwig, John F.
Journal of Organic Chemistry, 2009 , vol. 74, # 4 p. 1664 - 1672
反应条件
titanium tetrachloride; triphenylphosphine in tetrahydrofuran
T=60°C; 14 h;
参考文献
Kikuchi, Satoshi; Konishi, Hiroyuki; Hashimoto, Yukihiko
Tetrahedron, 2005 , vol. 61, # 14 p. 3587 - 3591
反应条件
tris-(o-tolyl)phosphine; sodium t-butanolate in tetrahydrofuran
T=20°C; 0.0833333 h; Inert atmosphere;
参考文献
Alvaro, Elsa; Hartwig, John F.
Journal of the American Chemical Society, 2009 , vol. 131, p. 7858 - 7868
反应条件
DiPPF; sodium t-butanolate in tetrahydrofuran
T=20°C; 2 h; Inert atmosphere;
参考文献
Alvaro, Elsa; Hartwig, John F.
Journal of the American Chemical Society, 2009 , vol. 131, p. 7858 - 7868
反应条件
silica gel; zirconium tetrachloride
T=50°C; 0.166667 h;
参考文献
Firouzabadi, Habib; Iranpoor, Nasser; Jafarpour, Maasoumeh
Tetrahedron Letters, 2006 , vol. 47, # 1 p. 93 - 97
反应条件
in tetrahydrofuran
T=-78°C; 4 h;
参考文献
Toste, F. Dean; Still, Ian W. J.
Tetrahedron Letters, 1995 , vol. 36, # 25 p. 4361 - 4364
反应条件
in diethyl ether; hexane
T=-10°C;
参考文献
Palumbo, Giovanni; Ferreri, Carla; D'Ambrosio, Clotilde; Caputo, Romualdo
Phosphorus and Sulfur and the Related Elements, 1984 , vol. 19, p. 235 - 238
反应条件
palladium diacetate; (R)-p-tol-BINAP; sodium t-butanolate in toluene
T=80°C; 24 h;
参考文献
Zheng, Nan; Christopher McWilliams; Fleitz, Fred J.; Armstrong III, Joseph D.; Volante
Journal of Organic Chemistry, 1998 , vol. 63, # 26 p. 9606 - 9607
反应条件
sulfuric acid
1 h; Ambient temperature;
参考文献
Nakazumi, Hiroyuki; Kitaguchi, Tooru; Ueyama, Tamio; Kitao, Teijiro
Synthesis, 1984 , # 6 p. 518 - 520
