1-(1,2-二氢-3-苊)乙酮合成路线 （共 11 条）
反应条件
aluminium trichloride in 1,2-dichloro-ethane
参考文献
Deady,L.W. et al.
Journal of Organic Chemistry, 1972 , vol. 37, p. 3335 - 3338
反应条件
1: acetyl chloride With AlCl3, aluminium chloride in dichloromethane
Friedel Crafts acylation; 0.25 h; Cooling with ice;
2: 1,2-dihydroacenaphthylene in dichloromethane
T=20°C; Friedel Crafts acylation; Cooling with ice;
参考文献
Xu, Chao; Luo, Wen-Feng; Li, Li-Jun; Yao, Shun; Song, Hang
Asian Journal of Chemistry, 2010 , vol. 22, # 5 p. 3923 - 3928
反应条件
hydrogen fluoride; acetic acid
参考文献
Fieser; Hershberg
Journal of the American Chemical Society, 1940 , vol. 62, p. 49,51
反应条件
boron trifluoride in dichloromethane
T=0 - 10°C; 1 h; Yields of byproduct given;
参考文献
Hyatt, John A.; Raynolds, Peter W.
Journal of Organic Chemistry, 1984 , vol. 49, # 2 p. 384 - 385
反应条件
[2,2']bipyridinyl; nickel dichloride; zinc in N,N-dimethyl acetamide
T=70°C; Dimerization; dehalogenation; 3 h;
参考文献
Adonin; Ryabinin; Starichenko
Russian Journal of Organic Chemistry, 1999 , vol. 35, # 6 p. 913 - 915
反应条件
in n-heptane
T=-78°C; 0.25 h;
参考文献
Eisch, John J.; Fichter, Kenneth C.
Journal of Organic Chemistry, 1984 , vol. 49, # 24 p. 4631 - 4639
反应条件
iodine; hypophosphorous acid in acetic acid
24 h; Heating;
参考文献
Fry, Albert J.; Allukian, Myron; Williams, Allison D.
Tetrahedron, 2002 , vol. 58, # 22 p. 4411 - 4415
反应条件
1: AlCl3 / CH2Cl2
2: 7 percent / NiCl2; 2,2'-bipyridyl; Zn / N,N-dimethyl-acetamide / 3 h / 70 °C
View Scheme
参考文献
Adonin; Ryabinin; Starichenko
Russian Journal of Organic Chemistry, 1999 , vol. 35, # 6 p. 913 - 915
反应条件
1: AlCl3 / CH2Cl2
2: Pd-C
View Scheme
参考文献
Perin,F. et al.
Bulletin de la Societe Chimique de France, 1971 , p. 1371 - 1378
反应条件
palladium on activated charcoal
参考文献
Perin,F. et al.
Bulletin de la Societe Chimique de France, 1971 , p. 1371 - 1378
